Forensic analysis of ignitable liquid using MonoTrap and its evaluation

I. Matsuoka, M. Kasamatsu, Hiromi Itamiya, Yasuhiro Suzuki
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Abstract

It is necessary to extract ignitable liquid residue from ˆre debris samples at scenes of arson using gasoline or kerosene as accelerants. Because extraction is essential for ˆre debris analysis and greatly in‰uences the composition of ignitable liquid residues, analysts have to understand the features of extraction methods and their proper conditions. To this purpose, we tested MonoTrap as an extraction method and then analyzed extracts by conducting gas chromatography mass spectrometry (GC/MS). We evaluated the eŠects of adsorption temperature, time, desorbing solvents, sample concentration, and the presence of water vapor on the composition of extracts. The result suggested that MonoTrap can be used successfully for forensic purposes and provided its proper conditions for extraction.
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MonoTrap法证可燃液体分析及其评价
在使用汽油或煤油作为助燃剂的纵火现场,有必要从re碎片样品中提取可燃液体残留物。由于提取对稀土碎屑分析至关重要,并且对可燃液体残留物的组成有很大影响,分析人员必须了解提取方法的特点及其适当的条件。为此,我们测试了MonoTrap作为提取方法,然后进行了气相色谱-质谱(GC/MS)分析。我们评估了eŠects吸附温度、时间、解吸溶剂、样品浓度和水蒸气对提取物组成的影响。结果表明MonoTrap可以成功地用于法医鉴定,并为提取提供了合适的条件。
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