Compaction and solid state sintering behavior of Cu-20%wt ZnO powders

M. Ardestani
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引用次数: 1

Abstract

In this research, compaction behavior and solid state sinterability of Cu-20wt.%ZnO powders were investigated. The compressibility of the powders was evaluated using Heckel and Panelli-Ambrosio equations. The powders were compacted uniaxially by 50, 100, 200 and 300 MPa at room temperature. The cold compacted powders were sintered at 850 and 1000◦C. The results showed that by increasing cold compaction pressure and sintering temperature the density of sintered compacts improved significantly. Additionally, it was found that the largest increase of density during sintering process was observed in the samples with relatively low green densities. The microstructural evaluation of the sintered samples by scanning electron microscopy (SEM) demonstrated that increasing the sintering temperature and cold compaction pressure resulted in decreasing the volume fraction of the pores and also their dimensions. However, it was confirmed that sintering temperature had more effective role on elimination of porosities rather than cold compaction pressure. The highest density was achieved for the samples which were compacted by 300 MPa and sintered at 1000◦C. K e y w o r d s: metal matrix composites (MMC), powder consolidation, sintering
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Cu-20%wt氧化锌粉体的压实和固态烧结性能
本文研究了Cu-20wt的压实性能和固态烧结性能。对氧化锌粉体进行了研究。采用Heckel方程和Panelli-Ambrosio方程对粉末的可压缩性进行了评价。在室温下对粉末进行50、100、200和300 MPa的单轴压实。冷压粉末在850℃和1000℃下烧结。结果表明,提高冷压压力和烧结温度,烧结坯的密度显著提高。在烧结过程中,绿密度相对较低的样品密度增加最大。通过扫描电镜(SEM)对烧结试样的微观结构进行了评价,结果表明,提高烧结温度和冷压压力,气孔的体积分数减小,气孔的尺寸减小。然而,证实了烧结温度比冷压压力对孔隙的消除作用更有效。在300 MPa压实和1000℃烧结的样品密度最高。金属基复合材料(MMC),粉末固结,烧结
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