THE INFLUENCE OF SILICA CALCINATION TEMPERATURE VARIATION TO THE HYDROPHOBICITY AND TRANSMITTANCE ON GLASS SUBSTRATE

Roihatur Rohmah, M. Zainuri
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Abstract

The hydrophobic surface can be self-cleaning. The hierarchy of surface roughness affects the hydrophobic surface. In this research, the hydrophobic surface was fabricated by modification of surface roughness from the composite filler. Natural silica was used as a filler and was done a variation of calcination temperature to modify the hierarchy of roughness formed. The variation of calcination temperature was 800°C, 1000°C, 1200°C, and 1400°C. The coating method was a dip-coating method by 30-second long immersion. A glass as coating media was coated by PVDF/SiO2 composite. The hydrophobic surface could be known from the value of the water contact angle (WCA) formed. If a water contact angle more than 90°, the surface could be called the hydrophobic surface. In this research, the hydrophobicity aspect cause of variation of calcination temperature was known from the value of water contact angle formed on the surface of PVDF/SiO2 composite coating 800°C, 1000°C, 1200°C, and 1400°C was 117,12° ± 0,98°, 107,80° ± 0,91°, 121,31° ± 1,45°, and 111,75° ± 1,47°, respectively.
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二氧化硅煅烧温度变化对玻璃基板疏水性和透光率的影响
疏水表面可自清洁。表面粗糙度的等级影响疏水表面。在本研究中,通过改性复合填料的表面粗糙度制备疏水表面。采用天然二氧化硅作为填料,通过改变煅烧温度来改变所形成的粗糙度等级。煅烧温度的变化范围为800℃、1000℃、1200℃、1400℃。涂布方法为长时间浸泡30秒的浸渍涂布法。采用PVDF/SiO2复合材料对玻璃进行涂覆。疏水表面可以通过形成的水接触角(WCA)值来判断。如果与水的接触角大于90°,则该表面可称为疏水表面。在本研究中,从800℃、1000℃、1200℃和1400℃时PVDF/SiO2复合涂层表面形成的水接触角值分别为117、12°±0、98°、107、80°±0、91°、121、31°±1、45°和111、75°±1、47°,了解了引起煅烧温度变化的疏水性方面。
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