The Effect of Immersion Time on Corrosion Rate on St37 Carbon Steel in 3% NaCl Corrosive Medium Using Waru Leaves Extract Inhibitor

Fredison Dian Sinaga, E. G. Suka, Pulung Karo Karo
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Abstract

The research of effect of immersion time on the corrosion rate of St37 carbon steel has been conducted in a 3% NaCl corrosive medium using a hibiscus leaves extract inhibitor. The samples of carbon steel St37 were immersed in a corrosive medium of NaCl 3% without being given and given the inhibitor of hibiscus leaf extract with a concentration of 15% for 3, 6, 9, and 12 days. Calculation of reduction in corrosion rate is carried out by the weight loss method. The results showed that adding the hibiscus leaves extract inhibitor effectively reduced the sample's corrosion rate with the most excellent efficiency at nine days immersion, which was equal to 78,48%. The results of XRD characterization show that the phase formed is pure Fe is a corrosion product. The results of SEM characterization showed that the surface microstructure of the sample after immersion was cracks, holes, and lumps, which indicated that the sample had been corroded. The results of EDS characterization show that in the soaked sample, there were corrosion products in the form of FeO compounds whose magnitude increased with every immersion.
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浸渍时间对3% NaCl腐蚀介质中St37碳钢腐蚀速率的影响
以木槿叶提取物为缓蚀剂,在3% NaCl腐蚀介质中,研究了浸泡时间对St37碳钢腐蚀速率的影响。碳钢St37样品在NaCl 3%的腐蚀性介质中浸泡3、6、9、12天,分别不给予和给予浓度为15%的木槿叶提取物抑制剂。采用失重法计算腐蚀速率的降低量。结果表明,加入木槿叶提取物缓蚀剂能有效降低样品的腐蚀速率,其中浸泡9 d时效果最佳,为78.48%。XRD表征结果表明,所形成的相为纯铁,为腐蚀产物。SEM表征结果表明,浸渍后试样的表面微观结构为裂纹、孔洞和块状,表明试样已被腐蚀。EDS表征结果表明,浸泡试样中存在FeO化合物形式的腐蚀产物,其强度随浸泡次数的增加而增加。
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