Synthesis of Multi-walled Carbon Nanotubes from Glycine Max Oil and Their Potential Applications

V.S. Angulakshmi, C. Sathiskumar, S. Karthikeyan
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Abstract

The discovery of carbon nanotubes has created new era in the field of nanotechnology. Spectacular properties of these nanostructured materials, stimulating scientists to peep into this tiny tube with ever increasing curiosity. The immediate challenge is to produce desired structural and characteristic featured carbon nanotubes in large quantities. Chemical vapor deposition is the most popular method of producing carbon nanotubes and it is of low-cost and highly useful technique for mass production of carbon nanotubes. These efforts requires not only chosen technique but also based on the precursor and the catalytic support. Glycine max oil a botanical hydrocarbon, has been found to be effective precursor for the synthesis of multi-walled carbon nanotubes (MWNTs) by Spray Pyrolysis over well dispersed Fe /Mo catalyst supported on silica at 650 °C under Ar atmosphere. As-grown MWNTs were characterized by SEM, HRTEM, Raman spectroscopy and Nitrogen adsorption studies. Raman spectroscopy revels that MWNTs are well graphitized. Dynamic and equilibrium studies of adsorption of Basic brown-4 on MWNTs were also reported.
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甘氨酸油合成多壁碳纳米管及其应用前景
碳纳米管的发现开创了纳米技术领域的新纪元。这些纳米结构材料的惊人特性,刺激着科学家们怀着越来越大的好奇心窥视这个微小的管道。当前的挑战是如何大量生产出结构和特性都符合要求的碳纳米管。化学气相沉积法是目前最常用的碳纳米管生产方法,是一种低成本、高实用的碳纳米管批量生产技术。这些工作不仅需要选择技术,而且需要基于前驱体和催化载体。摘要甘氨酸油是一种植物性烃类化合物,在分散良好的二氧化硅负载铁/钼催化剂上,在650℃氩气气氛下喷雾热解合成多壁碳纳米管(MWNTs)的有效前驱体。通过SEM、HRTEM、拉曼光谱和氮吸附研究对生长MWNTs进行了表征。拉曼光谱显示纳米碳管具有良好的石墨化特性。本文还报道了碱性棕-4在MWNTs上吸附的动态和平衡研究。
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来源期刊
Journal of Water and Environmental Nanotechnology
Journal of Water and Environmental Nanotechnology Materials Science-Materials Science (miscellaneous)
CiteScore
2.40
自引率
0.00%
发文量
0
审稿时长
8 weeks
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