Removing Water Blocking Damage in HTHP Tight Gas Reservoir Using Alternative Fracturing Fluid

Huifeng Liu, Jianli Zhang, Jiangyu Liu, Zhan-wei Yang, Tie Chen, Y. Gu, B. Baletabieke
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Abstract

Tight gas reservoir is easily damaged by liquid phase because of the small pores and throats in the formation. Hydraulic fracturing is usually used in this kind of reservoir to improve well productivity; however, sometimes the productivity declines instead of increasing after treatments because of the damage of the water-based stimulation fluids. This paper introduces a production decline case in the HTHP tight gas reservoir in Tarim Basin, Western China, and provides a new solution. Dixi gas reservoir belongs to the formation of Jurassic Ahe Group, with burial depth of about 5000m. The formation porosity is between 3.0-7.0%, and the permeability is less than 0.1mD. The average DST production rates of three wells in this area were more than 30×104 m3/d. However, the production declined by 40% after completion. Acidizing and proppant fracturing were both conducted to regain their productivities; however, the production rates were reduced even further after the treatments. One of these wells’ daily production rate declined by 78% compared to DST production after use of acid fracturing and hydraulic fracturing. A series of core flow tests were carried out to find out the causes and solutions. The results showed that the retention of fracturing fluid in the formation caused "water blocking damage", which leaded to a significant increase of water saturation and rapid decline of gas phase permeability. This is considered the main cause of well productivity decline. Therefore, minimizing the capillary force in the formation is considered the main approach to remove the damage. Three series of alternative fracturing fluids were developed and evaluated. The first one is fracturing fluid with methanol. 5%-20% methanol was added to the fracturing fluid to relieve water blocking damage. The results showed that most of the wells fractured by methanol fracturing fluid gained good post-fracturing productivity. Fluorocarbon surfactant fracturing fluid was also developed, in which the concentration of guar gum was reduced to 0.35% to decrease the residual damage. Experimental tests showed that its surface tension was reduced to 0.85mN/m, and the contact angle was increased to 65.47°. Besides, a new nano-scale additive was developed, which can reduce the surface tension of the fracturing fluid from 72.7mN/m to 30.0 mN/m, and increase the contact angle from 38.5° to 126.0°. Thus the capillary force was reduced from 91.78 kPa to -28.44 kPa. Core flow tests under reservoir conditions also showed that the flowback rate of the fracturing fluid with this nano-scale additive was increased by 15% and its displacement pressure was reduced by more than 50% compared with the fracturing fluid without this additive. Besides, the gas-phase permeability of core after treatment with this fracturing fluid was 30% higher than that of normal fracturing fluid. In this paper, the causes of water blocking damage in an HTHP tight gas reservoir during well stimulation were analyzed. Three sets of alternative fracturing fluids were introduced and their laboratory test results were illustrated. The field application of methanol fracturing fluid was also introduced, which showed a good function of water blocking removal effectiveness. The other two fluids are also expected to obtain effective results in the field.
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利用替代压裂液消除高温高压致密气藏水堵损害
致密气藏由于地层中孔隙和喉道较小,易受液相破坏。这类油藏通常采用水力压裂来提高油井产能;然而,有时由于水基增产液的破坏,产能在处理后反而下降而不是增加。本文介绍了塔里木盆地高温高压致密气藏的一个产量递减案例,并提出了新的解决方案。迪西气藏属于侏罗系阿河群组,埋深约5000m。地层孔隙度3.0 ~ 7.0%,渗透率小于0.1mD。该地区3口井DST平均产量均超过30×104 m3/d。然而,完工后产量下降了40%。为了恢复产能,进行了酸化和支撑剂压裂;然而,经过处理后,产量进一步降低。其中一口井的日产量与使用酸压裂和水力压裂后的DST产量相比下降了78%。进行了一系列岩心流动试验,找出了岩心流动的原因和解决方法。结果表明,压裂液在地层中的滞留造成“水堵损害”,导致含水饱和度显著升高,气相渗透率迅速下降。这被认为是导致油井产能下降的主要原因。因此,最小化地层中的毛细力被认为是消除损害的主要方法。开发并评价了三个系列的替代压裂液。第一个是含有甲醇的压裂液。在压裂液中加入5% ~ 20%的甲醇,以缓解水堵损害。结果表明,绝大多数采用甲醇压裂液压裂的井均获得了较好的压裂后产能。研制了氟碳表面活性剂压裂液,将瓜尔胶的浓度降至0.35%,以减少残余损伤。实验结果表明,其表面张力降低到0.85mN/m,接触角增加到65.47°。此外,开发出一种新型纳米级添加剂,可使压裂液表面张力从72.7mN/m降低到30.0 mN/m,接触角从38.5°增加到126.0°。因此毛细管力从91.78 kPa减小到-28.44 kPa。储层条件下的岩心流动测试也表明,与未添加纳米添加剂的压裂液相比,添加纳米添加剂的压裂液返排速率提高了15%,驱替压力降低了50%以上。经该压裂液处理后的岩心气相渗透率比常规压裂液提高30%。分析了高温高压致密气藏在增产改造过程中发生水堵的原因。介绍了三套替代性压裂液,并给出了室内试验结果。介绍了甲醇压裂液的现场应用情况,表明甲醇压裂液具有良好的除水堵效果。另外两种流体也有望在现场取得有效效果。
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