The growth of nickel ferrite single crystals

H. Makram, R. Krishnan
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引用次数: 1

Abstract

The mechanism of growth of nickel ferrite single crystals using the PbOPbF2 as the flux system, has been studied. The nucleation seems to start around 1170°C and the growth rate seems to be quite fast up to a temperature of 1100°C, as indicated by the yield and the size of the crystals obtained at this temperature. The growth rate then slows down appreciably.

The line width of 15 Oe along the 100 axis for the crystals thus obtained, indicate their good quality and a low content of Fe2+. By a thermal treatment, an ionic order is established among the sites and the resulting line width is 9 Oe. This value of 9 Oe for nickel ferrite is the lowest so far cited in the literature.

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镍铁氧体单晶的生长
研究了以PbO为助熔剂体系的铁氧体镍单晶的生长机理。在1170°C左右开始成核,直到1100°C时,生长速度似乎相当快,这可以从产率和在该温度下获得的晶体尺寸看出。然后增长速度明显放缓。所得晶体沿100轴的线宽为15 Oe,表明其质量好,Fe2+含量低。通过热处理,在位点之间建立了离子顺序,得到的线宽为9欧。镍铁氧体的9 Oe值是迄今为止文献中引用的最低值。
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