Surface degradation of nanocrystalline zirconia dental implants

V. Ocelík, U. Schepke, H. H. Rasoul, M. Cune, J. Hosson
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Abstract

Yttria-stabilized zirconia prepared by hot isostatic pressing represents attractive material for biomedical applications. In this work the degradation of yttria-stabilized zirconia dental implants abutments due to the tetragonal to monoclinic phase transformation after one year of clinical use was studied in detail. Microstructural characterization by Electron Back Scattering Diffraction was successfully applied. The amount and distribution of the monoclinic phase, the grain-size distribution and crystallographic orientations between tetragonal and monoclinic crystals in 3 mol.% yttria-stabilized polycrystalline zirconia were determined in two different types of abutments currently used in clinical practice. Clear crystallographic orientation relationship between parent tetragonal and daughter monoclinic phase was clearly observed. An important and novel conclusion is that no substantial bulk degradation of 3Y-TZP dental implant abutments was detected after 1 year of clinical use.
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纳米氧化锆牙种植体的表面降解
热等静压法制备的氧化钇稳定氧化锆是具有吸引力的生物医学材料。本文详细研究了氧化钇稳定氧化锆牙种植体基台在临床使用一年后由四方向单斜相变而降解的情况。成功地应用了电子背散射衍射法进行微结构表征。在目前临床使用的两种不同类型的基牙中,测定了3mol / %钇稳定多晶氧化锆中单斜相的数量和分布、四方晶和单斜晶之间的晶粒尺寸分布和晶体取向。清晰地观察到母方相和子单斜相之间的晶体取向关系。一个重要而新颖的结论是,临床使用1年后,没有检测到3Y-TZP牙种植基台的大量降解。
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