Preparation and characterisation of SnO–Fe2O3 nanocomposites

A. Subramaniyan, V. Veeraganesh
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引用次数: 2

Abstract

Nanocomposites are novel materials which are yet to be explored and utilised to its complete potential. Nanocomposites can be tailored by the volume fraction of the matrix, fibre and also by the size and shape of the nanophase material in the composite. Preparing nanocomposite with a desired shape and size remains a challenge. In the present work nanocomposites of SnO–Fe2O3.are prepared by a sol gel route with Ferric chloride and Tin chloride as precursors. The prepared nanocomposites are characterised by X-ray Diffraction(XRD), Ultraviolet Visible Spectroscopy (UV),Scanning Electron microscopy(SEM) and Fourier Transform Infrared Spectroscopy(FTIR). The crystallite size obtained is approximately 60 nm, with a band gap of 3.55 eV. The band gap of the composite could further be tuned with nanosize.
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SnO-Fe2O3纳米复合材料的制备与表征
纳米复合材料是一种有待开发和充分利用的新型材料。纳米复合材料可以根据基体、纤维的体积分数以及复合材料中纳米相材料的大小和形状来定制。制备具有理想形状和尺寸的纳米复合材料仍然是一个挑战。本文研究了SnO-Fe2O3纳米复合材料。以氯化铁和氯化锡为前驱体,采用溶胶-凝胶法制备。采用x射线衍射(XRD)、紫外可见光谱(UV)、扫描电镜(SEM)和傅里叶变换红外光谱(FTIR)对所制备的纳米复合材料进行了表征。所得晶体尺寸约为60 nm,带隙为3.55 eV。复合材料的带隙可以随着纳米尺寸的增大而进一步调整。
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