Comprehensive and heart-cutting multidimensional liquid chromatography-mass spectrometry and its applications in food analysis.

IF 6.9 2区化学 Q1 SPECTROSCOPY Mass Spectrometry Reviews Pub Date : 2023-04-03 DOI:10.1002/mas.21843

Irene Caño-Carrillo, Bienvenida Gilbert-López, Lidia Montero, Ana B Martínez-Piernas, Juan F García-Reyes, Antonio Molina-Díaz

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引用次数: 1

Abstract

In food analysis, conventional one-dimensional liquid chromatography methods sometimes lack sufficient separation power due to the complexity and heterogeneity of the analysed matrices. Therefore, the use of two-dimensional liquid chromatography (2D-LC) turns out to be a powerful tool to consider, especially when coupled to mass spectrometry (MS). This review presents the most remarkable 2D-LC-MS food applications reported in the last 10 years, including a critical discussion of the multiple approaches, modulation strategies as well as the importance of the optimisation of the different analytical aspects that will condition the 2D-LC-MS performance. The presence of contaminants in food (food safety), the food quality and authenticity or the relationship between the beneficial effects of food and human health are some of the fields in which most of the 2D-LC-MS applications are mainly focused. Both heart-cutting and comprehensive applications are described and discussed in this review, highlighting the potential of 2D-LC-MS for the analysis of such complex samples.

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全面切心多维液相色谱-质谱法及其在食品分析中的应用。

在食品分析中，由于被分析基质的复杂性和非均质性，传统的一维液相色谱法有时缺乏足够的分离能力。因此，使用二维液相色谱(2D-LC)被证明是一个强大的工具，特别是当与质谱(MS)相结合时。这篇综述介绍了过去10年来报道的最显著的2D-LC-MS食品应用，包括对多种方法的关键讨论，调制策略以及优化不同分析方面的重要性，这些分析方面将影响2D-LC-MS性能。食品中污染物的存在(食品安全)、食品质量和真实性或食品有益影响与人类健康之间的关系是大多数2D-LC-MS应用的主要领域。在这篇综述中描述和讨论了心脏切割和综合应用，强调了2D-LC-MS分析此类复杂样品的潜力。

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来源期刊

Mass Spectrometry Reviews 物理-光谱学

CiteScore

16.30

自引率

3.00%

发文量

期刊介绍： The aim of the journal Mass Spectrometry Reviews is to publish well-written reviews in selected topics in the various sub-fields of mass spectrometry as a means to summarize the research that has been performed in that area, to focus attention of other researchers, to critically review the published material, and to stimulate further research in that area. The scope of the published reviews include, but are not limited to topics, such as theoretical treatments, instrumental design, ionization methods, analyzers, detectors, application to the qualitative and quantitative analysis of various compounds or elements, basic ion chemistry and structure studies, ion energetic studies, and studies on biomolecules, polymers, etc.

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