加工食品中呋喃和烷基呋喃同时分析方法的研究进展

IF 0.2 4区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI:10.3358/shokueishi.64.29
Motoki Ogiso, Chihiro Hashimoto, Eisuke Toriumi, Kanako Nishimura, Seiichiro Iizuka, Kazuhiro Sakamoto, Yushi Yamamoto, Yukiko Yamada
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引用次数: 0

摘要

建立了顶空-气相色谱-质谱同时测定加工食品中烷基呋喃(呋喃、2-甲基呋喃、3-甲基呋喃和2,5-二甲基呋喃)的方法。呋喃、2-甲基呋喃、3-甲基呋喃和2,5-二甲基呋喃的单实验室验证数据具有良好的精密度和准确度。平均回收率为92 ~ 116%,中间精密度(RSDi)为0.9 ~ 12.9%。定量限分别为0.5 ~ 1.2 μg/kg(咖啡)、3.5 ~ 4.1 μg/kg(酱油)、0.4 ~ 1.3 μg/kg(其他食品:清苹果汁、婴儿配方奶粉和婴儿食品)。该方法对各种食品中痕量呋喃和烷基呋喃的检测灵敏度高,适用于食品安全风险管理监测。
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[Development for the Simultaneous Analytical Method of Furan and Alkyl Furans in Processed Foods].

A simultaneous analytical method was developed for the determination of alkyl furans (Furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran) in processed foods by headspace-GC-MS. Single-laboratory validation data of furan, 2-methylfuran, 3-methylfuran and 2,5-dimethylfuran showed good precision and accuracy. The mean recoveries ranged from 92 to 116%, the intermediate precision (RSDi) ranged from 0.9 to 12.9%. The level of LOQ ranged from 0.5 to 1.2 μg/kg (coffee), from 3.5 to 4.1 μg/kg (soy sauce), from 0.4 to 1.3 μg/kg (other foods: clear apple juice, infant formula and baby food), respectively. This method has the sensitivity to detect low levels of furan and alkyl furans contaminated in various foods and is thus applicable to surveillance for risk management in food safety.

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来源期刊
Food Hygiene and Safety Science
Food Hygiene and Safety Science Medicine-Public Health, Environmental and Occupational Health
CiteScore
0.70
自引率
0.00%
发文量
28
审稿时长
18-36 weeks
期刊介绍: Information not localized
期刊最新文献
[Analytical Method for Melengestrol Acetate in Livestock Products Using LC-MS/MS]. [Establishment of Rapid Simultaneous Analysis Method for Plant Toxins by LC-TOF-MS]. [Implementation and Evaluation of Risk Communication Regarding Residual Pesticides]. [Improved Indophenol Titration Method for Ascorbic Acid Using a Dropper and Electronic Balance: Enhanced Convenience and Efficiency]. [Comparison of DNA Extraction Methods for Processed Foods Containing Soybean or Maize].
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