微生物热解气相色谱法。不同热解参数对挥发性有机物产率的影响。

I Ericsson, L Larsson, P A Mårdh
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引用次数: 0

摘要

采用热解气相色谱法(PGC)对脆弱拟杆菌进行分析。研究了升温时间、热解温度和热解时间对挥发性有机热解产物收率的影响。采用短热解时间(8 msec)和高热解末端温度(1300℃)可获得高收率。在对试验生物的连续分析中,在所示热解条件下,挥发性有机产物总产率的标准差为+/- 7%。所描述的热解技术表明,热解碎片很少发生二次反应。
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Pyrolysis gas chromatography of microorganisms. Influence of various pyrolysis parameters on the yield of volatile organic products.

Bacteroides fragilis was analysed by pyrolysis gas chromatography (PGC). The influence of temperature rise time, pyrolysis temperature and pyrolysis time on the yield of volatile organic pyrolysis products was studied. The use of short pyrolysis time (8 msec) and a high pyrolysis end temperature (1300 degrees C) was found to provide a high yield. In consecutive analyses of the test organism, under the pyrolysis conditions indicated, the standard deviation of the total yield of volatile organic products was +/- 7%. The pyrolysis technique described suggests that few secondary reactions of the pyrolysis fragments occur.

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