涂层缺陷对氮化钛涂层钢疲劳强度的影响

K. Shiozawa, Toshinobu Tomosaka, Ling Han, Kou Motobayashi
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引用次数: 6

摘要

为研究涂层缺陷对疲劳强度的影响,采用PVD和CVD两种方法对涂层中有缺陷的0.37%C钢试样进行了空气和盐水(3.0% NaCl)中悬臂式旋转弯曲疲劳试验。试验前施加1.1-1.6%的静拉伸应变,导致试样表面涂层出现缺陷。涂层有缺陷的试样在两种环境下的疲劳寿命都明显低于未涂层和涂层无缺陷的试样。这种行为在空气中的疲劳中表现得很明显,即空气中的疲劳寿命降低了90-75%,而盐水溶液中的疲劳寿命降低了70-50%。虽然薄膜厚度为3 ~ 5 μm,但薄膜上的缺陷与在衬底上产生裂纹的缺口具有相同的作用。在空气疲劳的早期阶段,裂纹直接在基体下产生许多裂纹并合并成一个大裂纹。在腐蚀疲劳中,在疲劳过程的早期阶段,在缺陷下的基体上产生裂纹的腐蚀坑,而在形成坑之前的潜伏期不发生。
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Effect of Flaws in Coating Film on Fatigue Strength of Steel Coated with Titanium Nitride
To clarify the effect of flaws in the coating film on fatigue strength, cantilever-type rotating-bending fatigue tests were conducted in air and in saline solution (3.0% NaCl) using specimens of 0.37%C steel with flaws in the coating of titanium nitride (TiN)thin film coated by PVD and CVD methods. Flaws in the coating film on the specimen surface were introduced by the application of 1.1-1.6% static tensile strain before the test. An obvious decrease in fatigue life of the specimen with flawed coating film was observed in both environments, as compared with that of an uncoated specimen and a specimen with unflawed coating film. This behavior was marked for fatigue in air, that is, the decrease of fatigue life was 90-75% in air as opposed to 70-50% in saline solution. Although film thickness was 3-5 μm, the flaw in the film had the same effect as a notch at which cracks initiate on the substrate. Many cracks were induced in the substrate directly under a flaw and coalesced into a large crack at an early stage of fatigue in air. In corrosion fatigue, corrosion pits at which cracks initiate occur on the substrate under a flaw at an early stage of the fatigue process, and the incubation period prior to the formation of pits does not occur.
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