合成和描述NPP银(agn - nps)将龙皮提取物用作生物反应器

Rosman Parningotan, Y. Hamzah
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引用次数: 0

摘要

以红龙果皮提取物为生物载体,成功合成了银纳米粒子。合成过程是将硝酸银(AgNO3) 1mM溶液与红龙果皮提取物按1:5的体积比混合,然后加入几滴1M的NaOH溶液混合,直到溶液的pH值为10,然后对每个样品使用磁力搅拌器搅拌14分钟,然后培养。利用紫外可见光谱(UV-Vis)对样品进行了表征,得到了416 nm和2.98 eV的波长峰和能带隙。傅里叶变换红外光谱(FTIR)显示,在还原AgNO3中起作用的官能团有6个主要基团,其间隔为602-3427 cm-1。x射线衍射(XRD)光谱分析结果表明,该晶体尺寸为10.07-102.73 nm,具有面心立方(FCC)晶体结构,含有Ag2O杂质。从扫描电镜(SEM)图像可以看出,样品的形貌仍呈团块状。本研究结果表明,红龙果皮可将银离子还原为银纳米粒子。
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SINTESIS DAN KARAKTERISASI NPP PERAK (Ag-NPs) MENGGUNAKAN EKSTRAK KULIT BUAH NAGA SEBAGAI BIOREDUKTOR
Silver nanoparticle were successfully synthesized by using the red dragon fruit peel extract as a bioreductor. The synthesis process is mixed the solution of silver nitrate (AgNO3) 1mM and red dragon fruit peel extract with a volume ratio 1 : 5 and and then mixed with a few drops of NaOH solution 1M until the solution has a pH of 10 each and then stirred using magnetic stirrer for 14 minutes for each sample then incubator. The sample are characterized using the Ultra Violet Visible (UV-Vis) spectroscopy resulting in the wavelength peaks and energy band gap at 416 nm and 2.98 eV. A functional group that plays a role in reducting AgNO3 using the Fourier Transform Infra-Red Spectroscopy (FTIR) show six major groups that have interval of 602–3427 cm-1. The result of the X-Ray Diffraction (XRD) spectrum analysis saw a 10.07–102.73 nm crystal size with the Face Center Cubic (FCC) crystalline structure and have an Ag2O impurity. From Scanning Electron Microscope (SEM) image shows that morphology of sample is still agglomerated. The findings of the present research lead to conclusion that the red dragon fruit peel was found to reduced the silver ions to silver nanoparticle.
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