作为主动传感材料的氧化铁/聚苯胺/还原氧化石墨烯纳米复合材料的合成

Nurul Athirah Abu Hussein, H. F. Hawari, Y. H. Wong
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摘要

近年来,三元杂化材料因其独特的协同效应在各种应用中显示出提高器件性能的作用而受到广泛关注。本文合成了一种新型的三元杂化纳米复合材料- fe2o3 - PANI-RGO,并通过非原位法将其杂化成纳米复合材料。利用x射线衍射和红外光谱对合成的杂化纳米复合材料进行了理化表征。实验结果表明,杂化材料具有单独的材料峰,表明它们混合良好,并通过FTIR分析对官能团和振动模式进行了研究。由Debye-scherrer方程计算的晶粒尺寸表明材料为纳米级。还原氧化石墨烯材料对100ppm丙酮反应良好,反应时间为7.01 s,恢复时间为7.71s
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Synthesis of Iron Oxide/Polyaniline/Reduced Graphene Oxide Nanocomposite Materials as Active Sensing Material
Ternary hybrid materials have gained significant attention in recent years due to their unique synergistic effect shown to enhance the performance of devices in a variety of applications. In this present work, a novel ternary hybrid nanocomposite of ɣ-Fe2 O3 PANI-RGO was synthesized and hybrid together through ex-situ method to hybrid them into nanocomposite materials. The as-synthesized hybrid nanocomposite was subjected to physico-chemical characterization by x-ray diffraction and FTIR spectroscopy study. The experimental results observed that the hybrid materials have the individual material’s peak suggesting that they are blending well, and it was confirmed with FTIR analysis where the functional group and vibrational mode was studied. The crystallite size calculated from Debye-scherrer equation shows that the materials are in nano size. The RGO material shows a good responsive towards 100ppm acetone where the response and recovery time was 7.01 and 7.71s respectively
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