磁性液体的合成、表征及其在倾角传感器中的应用

Amit M. Dagade, P. V. Pillai, P. Goyal
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引用次数: 2

摘要

被称为铁磁流体的磁性液体是一种液体,作为一种智能材料,在磁场的存在下变得强磁化。本工作的目的是建立一种标准的、经济的氧化铁纳米颗粒的合成方法,并在其表面涂覆油酸,从而获得高质量的稳定铁磁流体。作者制备了悬浮在煤油中的纳米颗粒铁磁流体。为了避免聚集,纳米颗粒被油酸包裹。在目前的工作中,铁磁流体的稳定性从粒度、粒度分布和磁化等方面考虑。利用各种分析技术研究了最终流体的性质;利用x射线衍射(XRD)、透射电子显微镜(TEM)、傅里叶变换红外光谱(FTIR)等方法测定铁磁流体的原子间距离、颗粒的大小和形状以及油酸与纳米颗粒的粘附性等特性。考虑到铁磁流体的合成,剩下的部分工作致力于铁磁流体在倾角传感器中的应用。目前铁磁流体有许多商业应用,如癌症检测(MRI测试)、扬声器等。作为铁磁流体的应用之一,本文重点研究了基于铁磁流体的电感式倾角传感器的构建。我们研制的倾角传感器量程为±12°,分辨率为~±0.5°。
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Synthesis and characterization of magnetic liquid and its application as an inclination sensor
The magnetic liquid known as ferrofluid is a liquid, acts as a smart material, which becomes strongly magnetized in the presence of a magnetic field. The aim of this work to develop standard, economical method for synthesis of iron oxide nanoparticles along with their coating with oleic acid resulting in good quality of stable ferrofluid. The authors have prepared ferrofluid where nanoparticles are suspended in kerosene. To avoid aggregation, nanoparticles are coated with oleic acid. In present work, the stability of ferrofluid is considered in terms of particle size, size distribution and magnetization. The properties of final fluid are studied with the help of various analytical techniques; X-ray diffraction (XRD), Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR) which are used for the determination of characteristics of ferrofluid like interatomic distance, size and shape of the particles and adhesion of oleic acid to nanoparticles. In account of synthesized ferrofluid, remaining part of work is dedicated to application of ferrofluid in the inclination sensor. In present there are many commercial applications of ferrofluids such as cancer detection (MRI test), speakers etc. Here the focus is given to construct ferrofluid based inductive inclination sensor as one of the application of the ferrofluid. The range of inclination sensor developed by us is ±12° and the resolution is ~ ±0.5°.
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