{"title":"电流激活烧结共晶结构NiAl-34Cr和NiAl-28Cr-6Mo合金的高温腐蚀行为","authors":"C. Çeper, N. Ergin, Ö. Özdemir","doi":"10.21541/APJES.708253","DOIUrl":null,"url":null,"abstract":"In this study, NiAl-34Cr and NiAl-28Cr-6Mo eutectic alloys were produced by electric current assisted sintering (ECAS) method in a 3500-4200 A current range with a waiting time of 47 minutes. Phase examinations of the obtained samples were carried out with the help of X-ray diffraction analysis (XRD). While determining NiAl and Cr phases in NiAl-34Cr alloy from XRD patterns; It was determined that NiAl-28Cr-6Mo alloy consists of two phases, together with Mo residues, NiAl and CrMo. According to the Archimed principle, the relative density of NiAl-34Cr and NiAl-28Cr-6Mo alloys was determined as 96.2%, 97.9% respectively. The hardness values of NiAl-34Cr and NiAl-28Cr-6Mo samples were approximately 275 ± 13 HB and 255 ± 20 HB detected. In addition, the corrosion properties of the samples were examined by hot corrosion tests at 800, 900 and 1000°C for 165 hours (15 cycles) in 25% wt. K2SO4 + 75% wt. Na2SO4 salt medium. Weight changes, microstructure (SEM-EDS) and phase analysis of the samples after corrosion were carried out, and the corrosion properties of NiAl-34Cr alloy were found to be better compared to the Mo-added alloy. Ö ÖZDEMİR Academic Platform Journal of Engineering and Science 9-1, 79-85, 2021 80","PeriodicalId":294830,"journal":{"name":"Academic Platform Journal of Engineering and Science","volume":"493 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2021-01-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"High Temperature Corrosion Behavior of Eutectic Structured NiAl-34Cr and NiAl-28Cr-6Mo Alloys Produced by Electric Current Activated Sintering\",\"authors\":\"C. Çeper, N. Ergin, Ö. Özdemir\",\"doi\":\"10.21541/APJES.708253\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, NiAl-34Cr and NiAl-28Cr-6Mo eutectic alloys were produced by electric current assisted sintering (ECAS) method in a 3500-4200 A current range with a waiting time of 47 minutes. Phase examinations of the obtained samples were carried out with the help of X-ray diffraction analysis (XRD). While determining NiAl and Cr phases in NiAl-34Cr alloy from XRD patterns; It was determined that NiAl-28Cr-6Mo alloy consists of two phases, together with Mo residues, NiAl and CrMo. According to the Archimed principle, the relative density of NiAl-34Cr and NiAl-28Cr-6Mo alloys was determined as 96.2%, 97.9% respectively. The hardness values of NiAl-34Cr and NiAl-28Cr-6Mo samples were approximately 275 ± 13 HB and 255 ± 20 HB detected. In addition, the corrosion properties of the samples were examined by hot corrosion tests at 800, 900 and 1000°C for 165 hours (15 cycles) in 25% wt. K2SO4 + 75% wt. Na2SO4 salt medium. Weight changes, microstructure (SEM-EDS) and phase analysis of the samples after corrosion were carried out, and the corrosion properties of NiAl-34Cr alloy were found to be better compared to the Mo-added alloy. Ö ÖZDEMİR Academic Platform Journal of Engineering and Science 9-1, 79-85, 2021 80\",\"PeriodicalId\":294830,\"journal\":{\"name\":\"Academic Platform Journal of Engineering and Science\",\"volume\":\"493 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-01-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Academic Platform Journal of Engineering and Science\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.21541/APJES.708253\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Academic Platform Journal of Engineering and Science","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21541/APJES.708253","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
High Temperature Corrosion Behavior of Eutectic Structured NiAl-34Cr and NiAl-28Cr-6Mo Alloys Produced by Electric Current Activated Sintering
In this study, NiAl-34Cr and NiAl-28Cr-6Mo eutectic alloys were produced by electric current assisted sintering (ECAS) method in a 3500-4200 A current range with a waiting time of 47 minutes. Phase examinations of the obtained samples were carried out with the help of X-ray diffraction analysis (XRD). While determining NiAl and Cr phases in NiAl-34Cr alloy from XRD patterns; It was determined that NiAl-28Cr-6Mo alloy consists of two phases, together with Mo residues, NiAl and CrMo. According to the Archimed principle, the relative density of NiAl-34Cr and NiAl-28Cr-6Mo alloys was determined as 96.2%, 97.9% respectively. The hardness values of NiAl-34Cr and NiAl-28Cr-6Mo samples were approximately 275 ± 13 HB and 255 ± 20 HB detected. In addition, the corrosion properties of the samples were examined by hot corrosion tests at 800, 900 and 1000°C for 165 hours (15 cycles) in 25% wt. K2SO4 + 75% wt. Na2SO4 salt medium. Weight changes, microstructure (SEM-EDS) and phase analysis of the samples after corrosion were carried out, and the corrosion properties of NiAl-34Cr alloy were found to be better compared to the Mo-added alloy. Ö ÖZDEMİR Academic Platform Journal of Engineering and Science 9-1, 79-85, 2021 80
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