钛基复合材料的VHP制备与表征

K. S. Vadayar, S. Rani, G. Satya, V. V. B. Prasad
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引用次数: 2

摘要

不连续颗粒增强金属基复合材料(MMC)由于其成本低、易于制造和具有较好的各向同性力学性能,成为复合材料中主要而重要的应用类别之一。钛作为基体材料之一(其他重要的基体材料包括Al、Mg、Cu及其合金)因其高强度比、高刚度、良好的耐蚀性和高抗蠕变性而拓宽了其使用范围。本文采用粉末冶金方法,以不同粒径(165μm、49μm、8μm)的CP Ti粉(13μm)和B4C粉(165μm、49μm、8μm)为原料,制备了非连续增强钛基复合材料。混合后的粉体在1000℃下用VHP固结1hr。XRD分析证实了反应的程度和相的类型。进行了显微组织分析。通过三点弯曲试验对复合材料的强度进行了评价。试验结果表明,复合材料的抗弯强度高于未增强钛。利用扫描电镜对弯曲试样进行断口分析,发现复合材料呈混合型断裂
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Production and Characterization of Titanium Matrix Composites by VHP Route
Discontinuous particulate reinforced metal matrix composites (MMC)’s due to their low cost, ease of manufacturing and relatively good isotropic mechanical properties, form one of the major and important applicative class of composite materials. Titanium being one among the matrix materials (other important ones including Al, Mg, Cu and their alloys) widens its scope of usage due to its high strength to weight ratio, high stiffness, good corrosion resistance and high creep resistance. In the present work discontinuously reinforced titanium matrix composites (TMCs) were synthesized by using CP Ti powder (13μm) and B4C powder of varying particle sizes (165μm, 49μm, 8μm) through powder metallurgy. The blended powder were consolidated by VHP at 1000 ̊C for 1hr. XRD analysis was carried out to conform the extent of the reaction and the types of phases present. Microstructural analyses were carried out. The strength of the composites were evaluated by the three point bend test. The test revealed that the composites have high flexural strength with respect to unreinforced titanium. The fractography of the bend tested samples was carried out using SEM which revealed a mixed mode of fracture for the composites
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