铜在冷拔和强塑性变形后破碎带的形状和尺寸

N. Zemlyakova, S. Rogachev
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摘要

在这项工作中,采用实验方法研究了商业纯铜(m1级)经过两次冷(室温)拉伸和随后的等道角压剧烈塑性变形后的组织细化。本文介绍了在直径为20mm的样品的横截面上切割的薄片和箔片上经过4次和8次压道,每次压道后旋转90°(路线Bc)后测量结构部件的结果。用透射电镜对其结构进行了研究。为了比较微观结构在中观水平上的变化(小于我们使用扫描电子显微镜研究铜样品时获得的数据)。结果表明:在经过4道次和8道次后,形成了变形带——从长度上看与过渡带交替的碎片——具有位错结构的碎片。经过8次后,片段的平均尺寸约为300 nm。通过8道次剪切带的穿越,形成1.5 mm ~ 1.5 mm的菱形区域,其中位错较少的破碎变形带被过渡位错带和位错碎片所包围。宏观上看,经过4道次后得到的铜组织具有力学性能的各向异性。文中提出的铜在剧烈冷塑性变形后的结构组分的数值特征,使得在中尺度上理解结构细化方案成为可能。
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SHAPE AND DIMENSIONS OF FRAGMENTED BANDS AFTER COLD DRAWING AND INTENSE PLASTIC DEFORMATION OF THE COPPER
In this work, experimental methods were used to study the refinement of the structure of commercially pure copper (grade M 1) after double cold (at room temperature) plastic deformation by drawing and subsequent severe plastic deformation by equal channel angular pressing. The paper presents the results of measuring the structural components obtained on thin sections and foils cut from the cross-section of samples with a diameter of 20 mm after four and eight passes through the press channel with a 90° rotation after each pass (route Bc). A transmission electron microscope was used to study the structure. To compare changes in the microstructure at the mesolevel (less than we used the data obtained earlier in the study of copper samples using a scanning electron microscope. It is shown that after 4 passes and 8 passes, the deformation bands are formed – fragments (from in length), which alternate with transition bands – fragments with a dislocation structure. After 8 passes, the average size of the fragment was about 300 nm. As a result of crossing the shear bands in eight passes, diamond-shaped zones 1.5´1.5 mm was formed, in which fragmented deformation bands with less dislocation was surrounded by transition dislocation bands and fragments with dislocations. At the macro level, the copper structure obtained after 4 passes can have anisotropy of mechanical properties. The numerical characteristics of the structural components of copper after severe cold plastic deformation presented in the article make it possible to understand the structure refinement scheme at the mesoscale.
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