用扫描电镜(SEM)识别高温介质薄膜的击穿模式

S. Ul-Haq, G. Raju
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引用次数: 2

摘要

在本研究中,对25 /spl mu/m Kapton/spl reg/(聚酰亚胺)和Mylar/spl reg/聚酯(聚对苯二甲酸乙酯,PET)薄膜样品施加高压后,进行了直流击穿模式识别。在模式识别方面,采用扫描电子显微镜(SEM)技术获得150/spl倍/和300/spl倍/放大图像。在两幅图像中,击穿区域的形状几乎与电极的形状相同。SEM结果清楚地表明,在高压直流击穿过程中,Mylar/spl reg/聚酯的熔融过程比Kapton/spl reg/聚酰亚胺的熔融过程要快。在室温下,Mylar/spl reg/在直流击穿强度为326.7 MV/m时,观察到的孔直径约为265.5 /spl μ m,总影响面积为55.3/spl倍/10/sup -9/ m/sup 2/,而Kapton/spl reg/在击穿强度为364.9 MV/m时,观察到的孔直径为155.7 /spl μ m,总影响面积为19/spl倍/10/sup -9/ m/sup 2/。在这些薄膜中,使用了一种新型的环境室来测量电击穿强度。采用双参数威布尔分布对结果进行分析。
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Breakdown pattern identification in high temperature dielectric films using scanning electron microscopy (SEM)
In this research paper DC breakdown patterns identification were carried out after applying high voltages across samples of 25 /spl mu/m Kapton/spl reg/ (polyimide) and Mylar/spl reg/ polyester (poly(ethylene terephthalate), PET) films. For pattern identifications, Scanning Electron Microscopy (SEM) technique was employed for acquiring 150/spl times/ and 300/spl times/ magnified images. In both images the shape of breakdown area was almost identical to the shape of electrodes. The SEM results clearly revealed that the melting process during high voltage DC breakdown process is higher in case of Mylar/spl reg/ polyester than that of Kapton/spl reg/ (polyimide). In case of Mylar/spl reg/ at room temperature, observed hole diameter was approximately 265.5 /spl mu/m with the total effected area of 55.3/spl times/10/sup -9/ m/sup 2/ at DC breakdown strength of 326.7 MV/m as compared to Kapton/spl reg/, which was 155.7 /spl mu/m with total effected area of 19/spl times/10/sup -9/ m/sup 2/ at breakdown strength of 364.9 MV/m. In these films for the measurement of electrical breakdown strength a new type of environmental chamber was used. Two-parameter Weibull distribution has been used to analyze the results.
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