天蚕花梗乳胶合成纳米银及其光催化和抗菌活性研究

B. Venkataramana, S. Sankar, A. Saikumar, B. V. K. Naidu
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引用次数: 2

摘要

本文介绍了利用天然植物化学试剂绿色合成纳米银的方法。以天麻花梗为原料制备的水乳液作为还原剂和稳定剂。通过改变胶乳和AgNO3浓度以及反应时间来优化AgNPs的形成。紫外可见光谱分析表明,表面等离子体共振峰在350 ~ 450 nm之间,证实了银纳米粒子的形成。x射线粉末衍射分析显示AgNPs的结晶性质,傅里叶变换红外光谱分析显示AgNPs被多酚和其他芳烃稳定,而x射线能量色散光谱证实了AgNPs的金属性质。场发射扫描电镜和高分辨率透射电镜显示AgNPs的颗粒呈球形,动态光散射测得的AgNPs尺寸分布在40 ~ 50 nm范围内。合成的AgNPs具有降解/去除亚甲基蓝染料的光催化活性以及对铜绿假单胞菌、金黄色葡萄球菌和克雷伯菌的抑菌活性。
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Phytochemical Mediated Synthesis of Silver Nanoparticles using Musa paradisiaca Peduncle Latex and Its Photocatalytic and Antimicrobial Activity
In the present work, green synthesis of silver nanoparticles (AgNPs) using a natural phytochemical agent has been described. The aqueous latex from Musa paradisiaca peduncle has been utilized as reducing as well as stabilizing agent. The formation of AgNPs was optimized by varying latex and AgNO3 concentrations and finally reaction time. Ultraviolet-visible spectroscopic analysis showed the surface plasmon resonance peak between 350 and 450 nm confirms the formation of silver nanoparticles. X-ray powder diffraction analysis revealed the crystalline nature of AgNPs, Fourier transform infrared spectroscopy analysis revealed that AgNPs were stabilized by polyphenols and other aromatics present in the Musa Paradisiaca peduncle latex, while X-ray energy dispersive spectroscopy confirms the metallic nature. The field emission scanning electron microscopy and high resolution transmission electron microscopy showed the spherical shape of the particles and size distribution of AgNPs measured by dynamic light scattering which are in the range of 40 to 50 nm. The synthesized AgNPs showed photocatalytic activity on the degradation / removal of the methylene blue dye and the antimicrobial activity against Pseudomonas aeruginosa, Staphylococcus aureus and Klebseilla bacterial species.
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