石墨炉原子吸收光谱法(GF-AAS)测定白荆叶中铅

Z. A. Athaillah, Latifah Tulhusna, Nurlathifah, I. D. Dewijanti
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引用次数: 0

摘要

采用电热原子吸收光谱法(ET-AAS)测定了9种月桂叶样品中的铅浓度。采用磷酸铵作为基体改进剂,通过调整石墨炉(GF)设置,与不使用改进剂的方法相比,回收率为51.41 ~ 58.95%,精密度为18.45 ~ 26.02%,分析回收率为99.75 ~ 101.82%,精密度为4.09 ~ 5.21%。月桂叶中铅含量在0.78 mg/kg ~ 3.37 mg/kg之间。30%的样品超过了印度尼西亚食品和药物管理局为香料商品制定的最大限量(1.0 mg/kg),这一事实应鼓励进一步研究,重点是调查导致产品中铅含量高的因素和减轻这一问题的方法。提供给AIP Publishing的这篇文章的原始版本在作者的名字中包含一个错误。这个名字最初出现为latifatul Husna,但正确的名字是Latifah Tulhusna。本文的更新版本于2020年7月28日发布,更正了作者的姓名。
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Application of graphite furnace atomic absorption spectroscopy (GF-AAS) on determination of lead in bay (Syzygium polyanthum) leaves
Concentration of lead in nine bay leaf samples was determined using electrothermal atomic absorption spectrometry (ET-AAS). Utilization of ammonium phosphate as the matrix modifier and adjustment of graphite furnace (GF) setting has resulted in satisfactory analytical recovery (99.75 – 101.82%) and precision (4.09 – 5.21%), compared to that without modifier (recovery of 51.41 – 58.95% and precision of 18.45 – 26.02%). The lead content in bay leaves ranged between less than the detection limit (0.78 mg/kg) to 3.37 mg/kg. The fact that 30% samples exceeded the maximum limit (1.0 mg/kg) established by Indonesian Food and Drug Agency for spice commodities should encourage further study focusing on the investigation of factors that contributed to high lead content in the products and methods to mitigate the issue.The original version of this article supplied to AIP Publishing contained an error in the author’s name. The name originally appeared as, Latifahtul Husna, but the correct name is Latifah Tulhusna. An updated version of this article, with the author’s name corrected, was published on 28 July 2020.
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Preface: International Conference on Mathematical Sciences and Applications (ICMSA-2019) Third Hankel determinants for a certain subclass of analytic functions Numerical analysis of flow characteristics of Jeffery nanofluid past a moving plate in conducting field Power-law nanofluid on mixed convection with influence of double dispersion saturated non-Darcy porous media Application of graphite furnace atomic absorption spectroscopy (GF-AAS) on determination of lead in bay (Syzygium polyanthum) leaves
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