Al3+和Cr3+取代Ni-Zn-Cu铁氧体的结构、介电和磁性能

G. Satyanarayana, G. N. Rao, K. V. Babu
{"title":"Al3+和Cr3+取代Ni-Zn-Cu铁氧体的结构、介电和磁性能","authors":"G. Satyanarayana, G. N. Rao, K. V. Babu","doi":"10.30799/JNST.157.18040507","DOIUrl":null,"url":null,"abstract":"Ferrite materials with the general formula Ni0.7Zn0.2Cu0.1Fe1.9M0.1O4 (M=Al and Cr) are synthesized by using the solid state reaction method. X-ray diffraction (XRD), Fourier transforms infrared (FTIR) spectra, scanning electron microscope (SEM) dielectric measurements and vibrating sample magnetometer (VSM) techniques are utilized to study the various properties of the synthesized ferrites. XRD analysis confirmed the formation of single phase cubic spinel structure and the crystallite size is calculated by Scherrer’s formula found to be 20.3 and 12.5 nm. The magnetic properties were studied using pulse field hysteresis loop technique at room temperature. The saturation magnetization exhibit 98.71 and 91.69 emu/g for Al3+ and Cr3+ substituted Ni-Zn-Cu ferrites respectively. The magnetic permeability is increasing for chromium substituted compound in the frequency range 100 Hz to 120 MHz and significant modification in DC conductivity is explained on the basis of hopping mechanism.","PeriodicalId":268157,"journal":{"name":"Volume 4,Issue 5,2018","volume":"29 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2018-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Structural, Dielectric and Magnetic Properties of Al3+ and Cr3+ Substituted Ni-Zn-Cu Ferrites\",\"authors\":\"G. Satyanarayana, G. N. Rao, K. V. Babu\",\"doi\":\"10.30799/JNST.157.18040507\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Ferrite materials with the general formula Ni0.7Zn0.2Cu0.1Fe1.9M0.1O4 (M=Al and Cr) are synthesized by using the solid state reaction method. X-ray diffraction (XRD), Fourier transforms infrared (FTIR) spectra, scanning electron microscope (SEM) dielectric measurements and vibrating sample magnetometer (VSM) techniques are utilized to study the various properties of the synthesized ferrites. XRD analysis confirmed the formation of single phase cubic spinel structure and the crystallite size is calculated by Scherrer’s formula found to be 20.3 and 12.5 nm. The magnetic properties were studied using pulse field hysteresis loop technique at room temperature. The saturation magnetization exhibit 98.71 and 91.69 emu/g for Al3+ and Cr3+ substituted Ni-Zn-Cu ferrites respectively. The magnetic permeability is increasing for chromium substituted compound in the frequency range 100 Hz to 120 MHz and significant modification in DC conductivity is explained on the basis of hopping mechanism.\",\"PeriodicalId\":268157,\"journal\":{\"name\":\"Volume 4,Issue 5,2018\",\"volume\":\"29 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-08-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Volume 4,Issue 5,2018\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.30799/JNST.157.18040507\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Volume 4,Issue 5,2018","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30799/JNST.157.18040507","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3

摘要

采用固相反应法合成了通式为Ni0.7Zn0.2Cu0.1Fe1.9M0.1O4 (M=Al和Cr)的铁氧体材料。利用x射线衍射(XRD)、傅里叶变换红外(FTIR)光谱、扫描电镜(SEM)介电测量和振动样品磁强计(VSM)技术研究了合成铁氧体的各种性质。XRD分析证实形成了单相立方尖晶石结构,根据Scherrer公式计算晶粒尺寸分别为20.3 nm和12.5 nm。利用脉冲场磁滞回线技术研究了该材料在室温下的磁性能。Al3+和Cr3+取代Ni-Zn-Cu铁氧体的饱和磁化强度分别为98.71和91.69 emu/g。在100hz ~ 120mhz的频率范围内,铬取代化合物的磁导率增加,并根据跳变机理解释了其直流电导率的显著变化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Structural, Dielectric and Magnetic Properties of Al3+ and Cr3+ Substituted Ni-Zn-Cu Ferrites
Ferrite materials with the general formula Ni0.7Zn0.2Cu0.1Fe1.9M0.1O4 (M=Al and Cr) are synthesized by using the solid state reaction method. X-ray diffraction (XRD), Fourier transforms infrared (FTIR) spectra, scanning electron microscope (SEM) dielectric measurements and vibrating sample magnetometer (VSM) techniques are utilized to study the various properties of the synthesized ferrites. XRD analysis confirmed the formation of single phase cubic spinel structure and the crystallite size is calculated by Scherrer’s formula found to be 20.3 and 12.5 nm. The magnetic properties were studied using pulse field hysteresis loop technique at room temperature. The saturation magnetization exhibit 98.71 and 91.69 emu/g for Al3+ and Cr3+ substituted Ni-Zn-Cu ferrites respectively. The magnetic permeability is increasing for chromium substituted compound in the frequency range 100 Hz to 120 MHz and significant modification in DC conductivity is explained on the basis of hopping mechanism.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Design and Analysis of CMOS and CNTFET based Ternary Operators for Scrambling Preparation and Characterization of Transparent Conducting FTO Thin Films by Chemical Spray Pyrolysis Method Enhanced Sensing of 4-Nitroso-N,N–Dimethyl Aniline using Multi-Walled Carbon Nano Tube Modified Glassy Carbon Electrode Influence of pH and Temperature on The Structure and Size of Tin Oxide Nanoparticles Quantification of 4-Nitrophenol on Nanosize Polyaniline Modified Glassy Carbon Electrode through Electrochemical Method
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1