芥菜籽黏液的提取及特性研究

Bushra B. Jerad, R. M. Ali, A. A. Sahi
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摘要

从芥菜种子中分离出了芥菜黏液,并用热重法、超光速光速法等方法对其进行了鉴定。3种胶中含有不同官能团的x射线粉末、质子核磁共振、红外光谱,发现主要峰带分别属于OH(3410.15 ~ 3010.88)羟基、CH脂肪族(2925 ~ 2343.51)、C-O(1072.42 ~ 1060.85)基团和C=O 1743.65。对胶液的热化学参数进行了评价,并与标准胶液进行了比较,结果表明胶液在392℃下分解,质量损失55%;X射线处理发现胶液在19.9265°处有一个不尖锐的峰,最高53.35 cts,标准胶液在20.94°,19.04°处分别有不尖锐的峰,最高47.78,52.84 cts,核磁共振检查发现胶液中存在葡萄糖,鼠李糖,半乳糖醛酸,与两种标准胶相比含有相似的多糖。结果表明,芥菜胶在食品生产中具有良好的优势,可用于各种食品工业。
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EXTRACTION AND CHARACTERATION OF MUCILAGE EXTRACTED FROM MUSTARD SEEDS
The mucilage was isolated from mustard seeds and identification by some different methods like, thermo gravimetric, FTlR., X-ray powdered, proton NMR, FTIR spectra of the three gums contain different functional group in the gums, major peaks bands noticed were belong to OH (3410.15 – 3010.88) group from hydroxyl group, CH aliphatic (2925-2343.51), C-O (1072.42-1060.85) group and C=O 1743.65, Thermo chemical parameters of mucilage was evaluated and compared with the standard gums, Results indicated the mucilage was decomposed in 392°C and mass loss 55%, The X ray process found the mucilage had single not sharp peak at 19.9265°in highest 53.35 cts, Also the standard gums indicted not sharp peaks at 20.94°, 19.04°in highest 47.78, 52.84 cts separately, mucilage examination using nuclear magnetic resonance revealed the presence of glucose, rhamnose, galacturonic acid compared with two standard gums contain similar polysaccharide.lt was concluded The results that had that mucilage had good advantages, which might be used in various food industries showed that mustard gum is beneficial in food manufacturing.
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