采用点状脉冲电流逐层烧结方法对铜基和钛基金属粉末进行固结

Elkin Ia, Volkov Va, Stolbov Ks, Kolodkin Da, Chulkina Aa, Beltyukov An
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摘要

在本文中,我们提出了一种基于点脉冲烧结方法的导电粉末增材制造大块材料的技术。这种方法由粉末的逐层巩固组成,每一层都是由压缩在电极和衬底之间或电极和先前烧结层之间的小部分粉末连续烧结而形成的。使用所提出的方法,从具有不同化学成分(Cu, Ti,机械合金锡青铜)的粉末和各种形状(树枝状,哑铃状,石头状)的颗粒中获得大块样品。利用x射线衍射、电子显微镜和显微硬度测量,研究了获得的块状固结材料的结构相态和孔隙率。用这种方法烧结的粉末受到沿颗粒边界的热释放的很大影响,而热释放又取决于材料的电阻率。烧结试样的孔隙率主要取决于所用粉末的种类,并随着粉末颗粒尺寸的减小而减小。关键词:增材制造,电脉冲烧结,金属粉末,多孔结构
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Consolidation of Cu- and Ti-based metal powders using layer-by-layer, spot pulsed electric current sintering
In this paper, we propose a technique for additive manufacturing of bulk materials from electrically conductive powders, based on the method of point wise electro pulse sintering. This method consists of layer-by-layer consolidation of powders, each layer being formed as a result of successive sintering of small portions of powder compressed between the electrode and the substrate, or between the electrode and the previously sintered layer. Using the proposed method, bulk samples were obtained from powders having the different chemical composition (Cu, Ti, mechanically alloyed tin bronze), and particles of various shapes (dendritic, dumbbell, stone-shaped). Using X-ray diffraction, electron microscopy, and micro hardness measurements, the structural phase states, and porosity of the obtained bulk consolidated materials were studied. Sintering of powders using this method is greatly influenced by the heat release along the boundaries of the particles, which in turn depends on the electrical resistivity of the material. The porosity of the sintered samples mainly depends on the type of powder used and decreases with the decreasing size of the powder particles. Keywords: additive manufacturing, electro pulse sintering, metal powders, porous structure
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