超声空化等离子体放电与激光烧蚀法制备氧化铝纳米颗粒的比较研究

IF 1.3 Q4 NANOSCIENCE & NANOTECHNOLOGY Nanoscience and Technology-An International Journal Pub Date : 2023-01-01 DOI:10.1615/nanoscitechnolintj.2023049107
Nikolay Bulychev
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引用次数: 0

摘要

本文采用液体介质激光烧蚀和强超声空化作用下等离子体放电两种物理方法制备氧化铝纳米颗粒。采用动态光散射、扫描电镜、电动势测量等方法对两种方法制备的纳米颗粒进行了比较研究。结果表明,合成的颗粒呈球形,粒径约为50 ~ 70 nm,粒径分布较窄,具有较好的聚集沉降性能。通过测量纯粒子和水溶性聚合物聚乙二醇存在时的电动势值来检测纳米粒子的表面性质。本研究证明了超声波作用对颗粒表面活性的影响。
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A Comparative Study of Aluminum Oxide Nanoparticles Synthesized in Plasma Discharge under Ultrasonic Cavitation and by Laser Ablation
In this work, aluminum oxide nanoparticles were fabricated by two physical methods: laser ablation in liquid medium and plasma discharge under the action of intensive ultrasonic cavitation. The nanoparticles obtained by both methods were comparatively examined by the dynamic light scattering, scanning electron microscopy, electrokinetic potential measurements. It was found that the synthesized particles had spherical shape with size about 50-70 nm, relatively narrow particle size distribution and were stable to aggregation and sedimentation. The surface properties of nanoparticles were examined by the measurement of the electrokinetic potential values of pure particles as well as in the presence water-soluble polymer polyethylene glycol. This study allowed to demonstrate the effect of ultrasonic action on the particles surface activity.
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CiteScore
4.00
自引率
23.10%
发文量
20
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