{"title":"杂化法制备BST粉体及陶瓷","authors":"Thanawat Klaytae, Naratip Vittayakorn, Rattiphorn Sumang","doi":"10.1080/10584587.2023.2234571","DOIUrl":null,"url":null,"abstract":"AbstractBarium strontium titanate (Ba0.8Sr0.2TiO3; BST) ceramics, were prepared by the hybrid method between Solid-state reaction (SSR) and Sol-gel methods (SG) in a ratio of 1:0.1–1:0.5. The BST powder was successfully calcined at 850 °C for 2 h. This temperature is much lower than the calcination temperatures of the SSR method. The BST ceramics were sintered between 1150 and 1450 °C. All samples showed the pure perovskite structure corresponding to JCPDS no. 34-0411. The optimum sintering temperature was observed from the samples sintered at 1450 °C for 4 h, indicating a density of 5.26 g/cm3, dielectric constant of 7018, and ferroelectric properties: (Pmax = 13.8 μC/cm2, Pr = 2.5 μC/cm2 and Ec = 2.3 kV/cm at 30 kV/cm).Keywords: Phase transitionmicrostructureferroelectrichybrid method AcknowledgmentsThe authors thank the Program of Physics, Faculty of Science and Technology, Pibulsongkram Rajabhat University for supporting facilities.Disclosure StatementNo potential conflict of interest was reported by the author(s).Additional informationFundingThis research was funded by Pibulsongkram Rajabhat University, grant number RDI-2-61-14. This work received the best poster award from the International Conference and Exhibition on Science, Technology and Engineering of Materials [ISTEM2022].","PeriodicalId":13686,"journal":{"name":"Integrated Ferroelectrics","volume":"10 1","pages":"0"},"PeriodicalIF":0.7000,"publicationDate":"2023-09-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Preparation of BST Powders and Ceramics via a Hybrid Method\",\"authors\":\"Thanawat Klaytae, Naratip Vittayakorn, Rattiphorn Sumang\",\"doi\":\"10.1080/10584587.2023.2234571\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"AbstractBarium strontium titanate (Ba0.8Sr0.2TiO3; BST) ceramics, were prepared by the hybrid method between Solid-state reaction (SSR) and Sol-gel methods (SG) in a ratio of 1:0.1–1:0.5. The BST powder was successfully calcined at 850 °C for 2 h. This temperature is much lower than the calcination temperatures of the SSR method. The BST ceramics were sintered between 1150 and 1450 °C. All samples showed the pure perovskite structure corresponding to JCPDS no. 34-0411. The optimum sintering temperature was observed from the samples sintered at 1450 °C for 4 h, indicating a density of 5.26 g/cm3, dielectric constant of 7018, and ferroelectric properties: (Pmax = 13.8 μC/cm2, Pr = 2.5 μC/cm2 and Ec = 2.3 kV/cm at 30 kV/cm).Keywords: Phase transitionmicrostructureferroelectrichybrid method AcknowledgmentsThe authors thank the Program of Physics, Faculty of Science and Technology, Pibulsongkram Rajabhat University for supporting facilities.Disclosure StatementNo potential conflict of interest was reported by the author(s).Additional informationFundingThis research was funded by Pibulsongkram Rajabhat University, grant number RDI-2-61-14. This work received the best poster award from the International Conference and Exhibition on Science, Technology and Engineering of Materials [ISTEM2022].\",\"PeriodicalId\":13686,\"journal\":{\"name\":\"Integrated Ferroelectrics\",\"volume\":\"10 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.7000,\"publicationDate\":\"2023-09-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Integrated Ferroelectrics\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/10584587.2023.2234571\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"ENGINEERING, ELECTRICAL & ELECTRONIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Integrated Ferroelectrics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/10584587.2023.2234571","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"ENGINEERING, ELECTRICAL & ELECTRONIC","Score":null,"Total":0}
Preparation of BST Powders and Ceramics via a Hybrid Method
AbstractBarium strontium titanate (Ba0.8Sr0.2TiO3; BST) ceramics, were prepared by the hybrid method between Solid-state reaction (SSR) and Sol-gel methods (SG) in a ratio of 1:0.1–1:0.5. The BST powder was successfully calcined at 850 °C for 2 h. This temperature is much lower than the calcination temperatures of the SSR method. The BST ceramics were sintered between 1150 and 1450 °C. All samples showed the pure perovskite structure corresponding to JCPDS no. 34-0411. The optimum sintering temperature was observed from the samples sintered at 1450 °C for 4 h, indicating a density of 5.26 g/cm3, dielectric constant of 7018, and ferroelectric properties: (Pmax = 13.8 μC/cm2, Pr = 2.5 μC/cm2 and Ec = 2.3 kV/cm at 30 kV/cm).Keywords: Phase transitionmicrostructureferroelectrichybrid method AcknowledgmentsThe authors thank the Program of Physics, Faculty of Science and Technology, Pibulsongkram Rajabhat University for supporting facilities.Disclosure StatementNo potential conflict of interest was reported by the author(s).Additional informationFundingThis research was funded by Pibulsongkram Rajabhat University, grant number RDI-2-61-14. This work received the best poster award from the International Conference and Exhibition on Science, Technology and Engineering of Materials [ISTEM2022].
期刊介绍:
Integrated Ferroelectrics provides an international, interdisciplinary forum for electronic engineers and physicists as well as process and systems engineers, ceramicists, and chemists who are involved in research, design, development, manufacturing and utilization of integrated ferroelectric devices. Such devices unite ferroelectric films and semiconductor integrated circuit chips. The result is a new family of electronic devices, which combine the unique nonvolatile memory, pyroelectric, piezoelectric, photorefractive, radiation-hard, acoustic and/or dielectric properties of ferroelectric materials with the dynamic memory, logic and/or amplification properties and miniaturization and low-cost advantages of semiconductor i.c. technology.