(3E,5S,10S,13S,14S,17Z)-17-乙基-10,13-二甲基十六氢- 3h -环五[α]菲-3-一O-(甲基丙烯酰)肟C50H74N2O4的合成与晶体结构

IF 0.3 4区化学 Q4 CRYSTALLOGRAPHY Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-23 DOI:10.1515/ncrs-2023-0413

Peng Wei, Jin-Feng Zhao, Juan Zou, Jiang-Hai Ye, Kang He, Hong Xu

{"title":"(3E,5S,10S,13S,14S,17Z)-17-乙基-10,13-二甲基十六氢- 3h -环五[α]菲-3-一O-(甲基丙烯酰)肟C50H74N2O4的合成与晶体结构","authors":"Peng Wei, Jin-Feng Zhao, Juan Zou, Jiang-Hai Ye, Kang He, Hong Xu","doi":"10.1515/ncrs-2023-0413","DOIUrl":null,"url":null,"abstract":"Abstract C 50 H 74 N 2 O 4 , orthorhombic, P 1 (no. 1), a = 7.3320(3) Å, b = 11.8132(4) Å, c = 13.1604(5) Å, α = 99.1910(10)°, β = 95.039(1)°, γ = 95.8560(10)°, V = 1113.06(7) Å 3 , Z = 1, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1655, T = 273(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"29 5","pages":"0"},"PeriodicalIF":0.3000,"publicationDate":"2023-10-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α]phenanthren-3-one O-(methacryloyl) oxime, C50H74N2O4\",\"authors\":\"Peng Wei, Jin-Feng Zhao, Juan Zou, Jiang-Hai Ye, Kang He, Hong Xu\",\"doi\":\"10.1515/ncrs-2023-0413\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract C 50 H 74 N 2 O 4 , orthorhombic, P 1 (no. 1), a = 7.3320(3) Å, b = 11.8132(4) Å, c = 13.1604(5) Å, α = 99.1910(10)°, β = 95.039(1)°, γ = 95.8560(10)°, V = 1113.06(7) Å 3 , Z = 1, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1655, T = 273(2) K.\",\"PeriodicalId\":23792,\"journal\":{\"name\":\"Zeitschrift Fur Kristallographie-new Crystal Structures\",\"volume\":\"29 5\",\"pages\":\"0\"},\"PeriodicalIF\":0.3000,\"publicationDate\":\"2023-10-23\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Zeitschrift Fur Kristallographie-new Crystal Structures\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1515/ncrs-2023-0413\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CRYSTALLOGRAPHY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Zeitschrift Fur Kristallographie-new Crystal Structures","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1515/ncrs-2023-0413","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CRYSTALLOGRAPHY","Score":null,"Total":0}

引用次数: 0

摘要

摘要 C 50 H 74 N 2 O 4 , 正菱形, P 1 (No. 1), a = 7.3320(3) Å, b = 11.8132(4) Å, c = 13.1604(5) Å, α = 99.1910(10)°, β = 95.039(1)°, γ = 95.8560(10)°, V = 1113.06(7) Å 3 , Z = 1, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1655, T = 273(2) K。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文

微信好友朋友圈 QQ好友复制链接

本刊更多论文

Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α]phenanthren-3-one O-(methacryloyl) oxime, C₅₀H₇₄N₂O₄

Abstract C 50 H 74 N 2 O 4 , orthorhombic, P 1 (no. 1), a = 7.3320(3) Å, b = 11.8132(4) Å, c = 13.1604(5) Å, α = 99.1910(10)°, β = 95.039(1)°, γ = 95.8560(10)°, V = 1113.06(7) Å 3 , Z = 1, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1655, T = 273(2) K.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Zeitschrift Fur Kristallographie-new Crystal Structures 化学-晶体学

CiteScore

0.70

自引率

66.70%

发文量

326

审稿时长

5 months

期刊介绍： Zeitschrift für Kristallographie – New Crystal Structures was founded in 1997 as spin off of Zeitschrift für Kristallographie to meet the high demand to publish results of structure determination. All publications and their submitted CIF-data are online freely available (Open Access). Zeitschrift für Kristallographie – New Crystal Structures publishes results of determination of hitherto unknown crystal structures, and refinement of previously published crystal structures. Zeitschrift für Kristallographie – New Crystal Structures provides strict but constructive refereeing system, free access to submitted cif-files, Open Access to the PDF-files of publications, as well as data deposition at FIZ Karlsruhe and CCDC Cambridge.