溶液燃烧法合成掺镱ZnFe2O4尖晶石铁氧体的介电性能研究

Pub Date : 2023-01-01 DOI:10.56042/ijpap.v61i9.3841
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引用次数: 0

摘要

采用溶液燃烧法制备了一系列掺镱尖晶石铁素体ZnFe2O4。制备样品的XRD谱图证实了具有Fd-3m空间群的立方尖晶石结构。采用Scherrer公式计算样品的晶粒尺寸,分别为20.69 nm、17.16 nm和11.09 nm。扫描电镜图像显示形态分布不规则。研究了不同温度和频率下的介电常数和介电损耗。阻抗分析表明,导电机制与晶界电阻密切相关。
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Dielectric Study of Ytterbium Doped ZnFe2O4 Spinel Ferrite Synthesized by Solution Combustion Method
A series of ZnFe2O4 spinel ferrite doped with Ytterbium ions were synthesized using the solution combustion method. The XRD patterns of the prepared samples confirmed the cubic spinel structure with space group Fd-3m. Scherrer’s formula was used to calculate the crystallite size of the samples and it was found to be 20.69, 17.16 and11.09 nm. The SEM image showed irregular morphological distribution. The Dielectric constant and dielectric loss were studied at different temperatures and frequencies. The impedance analysis indicates that the conduction mechanism depends highly on the grain boundary resistance.
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