生姜提取物的植物化学、总酚和抗氧化活性及其在环保纳米银合成中的应用

Abdulkadir Mohammed Noori Jassim, Maryam Abdulghafor Ahmed, Salam A. H. Al-Ameri, Safana Ahmed Farhan, Omar M. Noori
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摘要

生姜(Zingiber Officinale)提取物含有许多成分和元素。生姜提取物可作为一种良好的生物还原剂制备纳米银。以生姜植物提取物为原料,用AgNO3合成AgNPs Green。绿色合成AgNPs是制备AgNPs的最佳开发方法,因为该方法比其他方法简单,环保且耗时少。通过UV-Vis、FTIR、AFM、SEM、Zeta电位和EDX对制备的AgNPs进行了表征。通过紫外可见分光光度法确定了合成AgNPs的最佳工艺条件。原子力显微镜(AFM)表征AgNPs的平均尺寸为53.45 nm,扫描电镜(SEM)表征其平均尺寸为21.91 ~ 33.79 nm。通过TLC和DPPH检测生姜的抗氧化和自由基清除活性,结果表明生姜具有较高的抗氧化和自由基清除活性,且活性随AgNPs的增加而增加。
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Phytochemical, Total Phenolic, and Antioxidant Activity of Ginger Extract and Its Use in the Synthesis of Eco-friendly Silver Nanoparticles
The Ginger (Zingiber Officinale) extract contain a lot of constituents and elements. Ginger extract can effort as a good bio-reductant to produce silver nanoparticles (AgNPs). The AgNPs Green synthesis was achieved by using the Ginger plant extract with AgNO3. The green synthesis of AgNPs is the best developing procedure for preparation, since this process is easier than other procedures, eco-friendly and fewer times consuming. The produced AgNPs were characterizing via UV-Vis, FTIR, AFM, SEM, Zeta potential and EDX. The optimal conditions for the synthesis AgNPs which was confirmed through UV–Vis spectrophotometer. Also, the AgNPs has been characterized by AFM with average size of 53.45 nm, SEM with average size of 21.91 to 33.79 nm. Antioxidant and free radical scavenge activity are examined through TLC and DPPH test, the results shows that the Ginger have a high activity, moreover, this activity increased with characterized AgNPs.
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