不同工艺改性义齿基托丙烯酸树脂的表面硬度评价

Inas Jawad, Ammar Qasim, Rizgar Hasan
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引用次数: 0

摘要

目的:评价热处理丙烯酸树脂经三种不同工艺改性后的表面硬度。材料和方法:采用以下方法对热固化丙烯酸树脂进行改性:(a)丙烯酸树脂与5%和10%的丙烯酸(AA)共聚,(b)加入5%和10%的热活化氧化锌(ZnO), (c)将锌离子通过有机链接(5%和10%的二丙烯酸锌(ZDA))化学键合或接合到聚合物链中,得到共聚物。丙烯酸样品的尺寸为(30,15和3)±0.2 mm。表面硬度用硬度计(邵氏D)硬度计测定。结果:实验组(改性组)表面硬度均有提高。与对照组和其余改性样品相比,10% ZnO和10% ZDA改性的丙烯酸基团的硬度均有统计学上的显著增加。结论:两种工艺均能显著提高热固化丙烯酸树脂的硬度;通过加入10%重量的热活化ZnO或与10%重量的ZDA共聚得到聚甲基丙烯酸甲酯-丙烯酸锌共聚物。
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Evaluation of Surface hardness of Denture Base Acrylic Resin Modified with Different Techniques
Aims: Evaluation of the surface hardness of heat-treated acrylic resin after modifying it with three different techniques. Materials and Methods: Heat cured acrylic resin was modified by: (a) The copolymerization of acrylic resin with 5% and 10% of acrylic acid (AA), (b) The addition of 5% and 10% thermally activated zinc oxide (ZnO) and (c) The chemical bonding or engagement of Zinc ions into the polymer chain by an organic link, zinc diacrylate (ZDA) in 5% and 10%, to get a copolymer. The acrylic specimens have dimensions of (30, 15 and 3) ± 0.2 mm. Surface hardness was determined using a Durometer (Shore D) hardness tester. Results: There was general increase of the surface hardness of the experimental (modified) groups. A statical significant increase in the hardness of both acrylic groups modified by 10% ZnO and 10% ZDA compared to the control group and the remaining modified samples. Conclusion: Two techniques had significantly improved the hardness of heat cured acrylic resin; either by adding 10% by weight of thermally activated ZnO or by copolymerizing it with 10% by weight of ZDA to get poly (methyl methacrylate -co-zinc acrylate) copolymer.
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发文量
34
审稿时长
10 weeks
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