儿茶素和纳米壳聚糖对聚乳酸/聚乳酸共混包装膜中菌落减少和材料性能的影响

Suryani Salim, Teuku Rihayat, None Fitria, Aida Safitri
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引用次数: 0

摘要

石油化工聚合物基塑料的广泛使用带来了重大的环境挑战。一个可行的解决方案是结合高质量的生物材料作为传统塑料的替代品。为实现这一目标,将聚乳酸(PLA)和聚己内酯(PCL)生物聚合物与儿茶素和纳米壳聚糖添加剂相结合,创新食品包装材料。该工艺涉及使用螺杆挤出机进行混合和熔化。样品配方采用PLA聚合物(9.5 g)和PCL (0.5 g)的组合,儿茶素(0%、5%、10%、15%、20%、25%和30%)和纳米壳聚糖(5%、10%、15%、20%、25%和30%)的浓度变化。通过抗拉强度测试、FTIR分析和菌落还原,样品SA4达到了最高的抗拉强度,为45.10 MPa。FT-IR分析显示,PLA/PCL基体共混物中存在N-H、C- h、C=O和C-O等官能团,表明PLA/PCL基体共混物与纳米壳聚糖和儿茶素添加剂组分之间成功相互作用。值得注意的是,样品SA4在保存24小时后金黄色葡萄球菌菌落显著减少96%。
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THE EFFECT OF CATECHINS AND NANOCHITOSAN ON REDUCING BACTERIAL COLONIES AND MATERIAL PERFORMANCE IN PACKAGING FILMS BASED ON PLA/PCL BLEND
The extensive utilization of petrochemical polymer-based plastics has led to significant environmental challenges. A viable solution involves the incorporation of high-quality biomaterials as a substitute for traditional plastics. In pursuit of this goal, Polylactic Acid (PLA) and Polycaprolactone (PCL) biopolymers were combined with catechin and nano chitosan additives to innovate food packaging materials. The process involved the utilization of a screw extruder for mixing and melting. The sample formulation employed a combination of PLA polymer (9.5 g) and PCL (0.5 g). The variations in catechin (0%, 5%, 10%, 15%, 20%, 25%, and 30%), while nano chitosan was added in concentrations (5%, 10%, 15%, 20%, 25%, and 30%). The highest tensile strength recorded, at 45.10 MPa, was achieved by sample SA4, as indicated by tensile strength testing, FTIR analysis, and colony reduction. FT-IR analysis revealed the presence of functional groups, namely N-H, C-H, C=O, and C-O, signifying successful interactions between the PLA/PCL matrix blend and the additive components of nanochitosan and catechins. Remarkably, sample SA4 exhibited a remarkable 96% reduction in S. aureus bacterial colonies following 24 hours of storage.
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