Heronilton Mendes de Lira, Wésia Amanda de Oliveira Barbosa, Euclides Apolinário Cabral de Pina, Alexandre Douglas Araújo de Moura, Pilar Rey Rodriguez, Ivanilda Ramos de Melo, Oscar Olímpio de Araújo Filho
{"title":"高能球磨和热挤压法制备SiC、TiN、ZnO纳米颗粒增强AA7075铝合金复合材料","authors":"Heronilton Mendes de Lira, Wésia Amanda de Oliveira Barbosa, Euclides Apolinário Cabral de Pina, Alexandre Douglas Araújo de Moura, Pilar Rey Rodriguez, Ivanilda Ramos de Melo, Oscar Olímpio de Araújo Filho","doi":"10.1590/1980-5373-mr-2023-0154","DOIUrl":null,"url":null,"abstract":"In this work, composite powders of aluminum alloy 7075 (AA7075) reinforced by 2 weight percent of nanosized particles of silicon carbide (SiC), titanium nitride (TiN), and zinc oxide (ZnO) were produced in a bath of isopropyl alcohol by high energy ball milling during 480 min at 25 ºC, 900 rpm, and Balls-to-Powder Weight Ratio (BPR) of 20:1. The techniques of X-Ray Diffraction (XRD), Laser Diffraction Method (LDM), Scanning Electron Microscopy (SEM), and microanalysis of Energy Dispersive Spectroscopy (EDS) were used to characterize the powders as received and processed. Then, the composites were hot extruded and characterized by XRD, SEM, and microhardness Vickers (HV). The milling process reduces the crystallite and particle size to around 30 nm and 10 µm, respectively. After extrusion, a fine microstructure and good consolidation were found for all bars, except for AA7075 as received. The ranging microhardness values were from 97 HV to 121 HV.","PeriodicalId":18331,"journal":{"name":"Materials Research-ibero-american Journal of Materials","volume":"134 1","pages":"0"},"PeriodicalIF":1.5000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Manufacturing of AA7075 Aluminum Alloy Composites Reinforced by Nanosized Particles of SiC, TiN, and ZnO by High-Energy Ball Milling and Hot Extrusion\",\"authors\":\"Heronilton Mendes de Lira, Wésia Amanda de Oliveira Barbosa, Euclides Apolinário Cabral de Pina, Alexandre Douglas Araújo de Moura, Pilar Rey Rodriguez, Ivanilda Ramos de Melo, Oscar Olímpio de Araújo Filho\",\"doi\":\"10.1590/1980-5373-mr-2023-0154\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this work, composite powders of aluminum alloy 7075 (AA7075) reinforced by 2 weight percent of nanosized particles of silicon carbide (SiC), titanium nitride (TiN), and zinc oxide (ZnO) were produced in a bath of isopropyl alcohol by high energy ball milling during 480 min at 25 ºC, 900 rpm, and Balls-to-Powder Weight Ratio (BPR) of 20:1. The techniques of X-Ray Diffraction (XRD), Laser Diffraction Method (LDM), Scanning Electron Microscopy (SEM), and microanalysis of Energy Dispersive Spectroscopy (EDS) were used to characterize the powders as received and processed. Then, the composites were hot extruded and characterized by XRD, SEM, and microhardness Vickers (HV). The milling process reduces the crystallite and particle size to around 30 nm and 10 µm, respectively. After extrusion, a fine microstructure and good consolidation were found for all bars, except for AA7075 as received. The ranging microhardness values were from 97 HV to 121 HV.\",\"PeriodicalId\":18331,\"journal\":{\"name\":\"Materials Research-ibero-american Journal of Materials\",\"volume\":\"134 1\",\"pages\":\"0\"},\"PeriodicalIF\":1.5000,\"publicationDate\":\"2023-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Research-ibero-american Journal of Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1590/1980-5373-mr-2023-0154\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Research-ibero-american Journal of Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1590/1980-5373-mr-2023-0154","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Manufacturing of AA7075 Aluminum Alloy Composites Reinforced by Nanosized Particles of SiC, TiN, and ZnO by High-Energy Ball Milling and Hot Extrusion
In this work, composite powders of aluminum alloy 7075 (AA7075) reinforced by 2 weight percent of nanosized particles of silicon carbide (SiC), titanium nitride (TiN), and zinc oxide (ZnO) were produced in a bath of isopropyl alcohol by high energy ball milling during 480 min at 25 ºC, 900 rpm, and Balls-to-Powder Weight Ratio (BPR) of 20:1. The techniques of X-Ray Diffraction (XRD), Laser Diffraction Method (LDM), Scanning Electron Microscopy (SEM), and microanalysis of Energy Dispersive Spectroscopy (EDS) were used to characterize the powders as received and processed. Then, the composites were hot extruded and characterized by XRD, SEM, and microhardness Vickers (HV). The milling process reduces the crystallite and particle size to around 30 nm and 10 µm, respectively. After extrusion, a fine microstructure and good consolidation were found for all bars, except for AA7075 as received. The ranging microhardness values were from 97 HV to 121 HV.