高能球磨和热挤压法制备SiC、TiN、ZnO纳米颗粒增强AA7075铝合金复合材料

IF 1.5 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Research-ibero-american Journal of Materials Pub Date : 2023-01-01 DOI:10.1590/1980-5373-mr-2023-0154
Heronilton Mendes de Lira, Wésia Amanda de Oliveira Barbosa, Euclides Apolinário Cabral de Pina, Alexandre Douglas Araújo de Moura, Pilar Rey Rodriguez, Ivanilda Ramos de Melo, Oscar Olímpio de Araújo Filho
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引用次数: 0

摘要

在异丙醇浴中,在25℃、900转/分、480 min的高能球磨条件下,以2%的纳米碳化硅(SiC)、氮化钛(TiN)和氧化锌(ZnO)增强7075铝合金(AA7075)复合粉末,球粉重量比(BPR)为20:1。采用x射线衍射(XRD)、激光衍射法(LDM)、扫描电镜(SEM)和能谱分析(EDS)等技术对粉末进行了表征。然后对复合材料进行热挤压,并用XRD、SEM和显微硬度维氏(HV)对其进行表征。铣削过程将晶粒和颗粒尺寸分别减小到30 nm和10 μ m左右。挤压后,除了收到的AA7075外,所有棒材都有良好的组织和固结。显微硬度范围为97 ~ 121 HV。
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Manufacturing of AA7075 Aluminum Alloy Composites Reinforced by Nanosized Particles of SiC, TiN, and ZnO by High-Energy Ball Milling and Hot Extrusion
In this work, composite powders of aluminum alloy 7075 (AA7075) reinforced by 2 weight percent of nanosized particles of silicon carbide (SiC), titanium nitride (TiN), and zinc oxide (ZnO) were produced in a bath of isopropyl alcohol by high energy ball milling during 480 min at 25 ºC, 900 rpm, and Balls-to-Powder Weight Ratio (BPR) of 20:1. The techniques of X-Ray Diffraction (XRD), Laser Diffraction Method (LDM), Scanning Electron Microscopy (SEM), and microanalysis of Energy Dispersive Spectroscopy (EDS) were used to characterize the powders as received and processed. Then, the composites were hot extruded and characterized by XRD, SEM, and microhardness Vickers (HV). The milling process reduces the crystallite and particle size to around 30 nm and 10 µm, respectively. After extrusion, a fine microstructure and good consolidation were found for all bars, except for AA7075 as received. The ranging microhardness values were from 97 HV to 121 HV.
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来源期刊
Materials Research-ibero-american Journal of Materials
Materials Research-ibero-american Journal of Materials MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
2.40
自引率
11.80%
发文量
161
审稿时长
3 months
期刊介绍: Information not localized
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