{"title":"氢对05Kh13N8M3铸马氏体钢静态抗裂性能的影响","authors":"O. I. Balytskyi, L. M. Ivaskevych","doi":"10.1007/s11223-023-00581-w","DOIUrl":null,"url":null,"abstract":"<p>The laws governing the influence of a hydrogen atmosphere at a pressure of up to 15 MPa with controlled total oxygen and water vapor content of up to 0.004 g/m<sup>3</sup> and pre-absorbed hydrogen on the strength and ductility characteristics, short-term and long-term static crack resistance of 05Kh13N8M3 cast martensitic steel (in wt.%: 0.045 C, 0.38 Si, 12.9 Cr, 2.69 Mo, 0.43 Mn, 7.8 Ni, 0.057 La) at room temperature were studied. After hydrogen pre-charging for 4 h at a temperature of 773 K and a pressure of 5, 10, and 15 MPa, the hydrogen content of the specimens determined with a LECO TCH 600 device by infrared adsorption with melting was 3.3, 4.9, and 7.6 ppm, respectively. It was found that under short-term loading, the intensity of the effect of hydrogen on the fracture toughness of steel increases with an increase in the absorbed hydrogen content, crack sharpness, and a decrease in the loading rate. At the maximum hydrogen concentration of 7.6 ppm and a tensile rate of 0.1 mm/min, the relative elongation, lateral contraction ratio of smooth 25 mm long cylindrical specimens with a test portion diameter of 5 mm and the critical stress intensity factor of beam specimens measuring 20×10×100 mm with a relative length of the pre-induced crack of <span>\\(\\upvarepsilon =\\)</span> 0.53 decrease almost twofold. At the same concentration, hydrogen does not affect the stress intensity factor of cracked specimens at a rate of 10 mm/min and specimens with a stress concentrator in the form of a notch with a tip radius of 0.065 mm at a rate of 0.1 mm/min. Under long-term static loading with a test duration of 300 h of double-cantilever beam specimens in the form of a rectangular plate 10 mm thick with milled grooves 3 mm deep and a tip angle of 60°, the threshold value of the stress intensity factor decreases. The rate of subcritical crack growth in the second portion of the hydrogen cracking diagram increases in proportion to the logarithm of hydrogen concentration.</p>","PeriodicalId":22007,"journal":{"name":"Strength of Materials","volume":null,"pages":null},"PeriodicalIF":0.7000,"publicationDate":"2023-12-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of Hydrogen on the Static Crack Resistance of 05Kh13N8M3 Cast Martensitic Steel\",\"authors\":\"O. I. Balytskyi, L. M. Ivaskevych\",\"doi\":\"10.1007/s11223-023-00581-w\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The laws governing the influence of a hydrogen atmosphere at a pressure of up to 15 MPa with controlled total oxygen and water vapor content of up to 0.004 g/m<sup>3</sup> and pre-absorbed hydrogen on the strength and ductility characteristics, short-term and long-term static crack resistance of 05Kh13N8M3 cast martensitic steel (in wt.%: 0.045 C, 0.38 Si, 12.9 Cr, 2.69 Mo, 0.43 Mn, 7.8 Ni, 0.057 La) at room temperature were studied. After hydrogen pre-charging for 4 h at a temperature of 773 K and a pressure of 5, 10, and 15 MPa, the hydrogen content of the specimens determined with a LECO TCH 600 device by infrared adsorption with melting was 3.3, 4.9, and 7.6 ppm, respectively. It was found that under short-term loading, the intensity of the effect of hydrogen on the fracture toughness of steel increases with an increase in the absorbed hydrogen content, crack sharpness, and a decrease in the loading rate. At the maximum hydrogen concentration of 7.6 ppm and a tensile rate of 0.1 mm/min, the relative elongation, lateral contraction ratio of smooth 25 mm long cylindrical specimens with a test portion diameter of 5 mm and the critical stress intensity factor of beam specimens measuring 20×10×100 mm with a relative length of the pre-induced crack of <span>\\\\(\\\\upvarepsilon =\\\\)</span> 0.53 decrease almost twofold. At the same concentration, hydrogen does not affect the stress intensity factor of cracked specimens at a rate of 10 mm/min and specimens with a stress concentrator in the form of a notch with a tip radius of 0.065 mm at a rate of 0.1 mm/min. Under long-term static loading with a test duration of 300 h of double-cantilever beam specimens in the form of a rectangular plate 10 mm thick with milled grooves 3 mm deep and a tip angle of 60°, the threshold value of the stress intensity factor decreases. The rate of subcritical crack growth in the second portion of the hydrogen cracking diagram increases in proportion to the logarithm of hydrogen concentration.</p>\",\"PeriodicalId\":22007,\"journal\":{\"name\":\"Strength of Materials\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.7000,\"publicationDate\":\"2023-12-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Strength of Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1007/s11223-023-00581-w\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Strength of Materials","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1007/s11223-023-00581-w","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
引用次数: 0
摘要
研究了压力为15 MPa、总氧和水蒸气含量控制在0.004 g/m3以下和预吸收氢对05Kh13N8M3铸造马氏体钢(wt)强度和延展性特性、短期和长期静态抗裂性能的影响规律。%: 0.045 C, 0.38 Si, 12.9 Cr, 2.69 Mo, 0.43 Mn, 7.8 Ni, 0.057 La) at room temperature were studied. After hydrogen pre-charging for 4 h at a temperature of 773 K and a pressure of 5, 10, and 15 MPa, the hydrogen content of the specimens determined with a LECO TCH 600 device by infrared adsorption with melting was 3.3, 4.9, and 7.6 ppm, respectively. It was found that under short-term loading, the intensity of the effect of hydrogen on the fracture toughness of steel increases with an increase in the absorbed hydrogen content, crack sharpness, and a decrease in the loading rate. At the maximum hydrogen concentration of 7.6 ppm and a tensile rate of 0.1 mm/min, the relative elongation, lateral contraction ratio of smooth 25 mm long cylindrical specimens with a test portion diameter of 5 mm and the critical stress intensity factor of beam specimens measuring 20×10×100 mm with a relative length of the pre-induced crack of \(\upvarepsilon =\) 0.53 decrease almost twofold. At the same concentration, hydrogen does not affect the stress intensity factor of cracked specimens at a rate of 10 mm/min and specimens with a stress concentrator in the form of a notch with a tip radius of 0.065 mm at a rate of 0.1 mm/min. Under long-term static loading with a test duration of 300 h of double-cantilever beam specimens in the form of a rectangular plate 10 mm thick with milled grooves 3 mm deep and a tip angle of 60°, the threshold value of the stress intensity factor decreases. The rate of subcritical crack growth in the second portion of the hydrogen cracking diagram increases in proportion to the logarithm of hydrogen concentration.
Effect of Hydrogen on the Static Crack Resistance of 05Kh13N8M3 Cast Martensitic Steel
The laws governing the influence of a hydrogen atmosphere at a pressure of up to 15 MPa with controlled total oxygen and water vapor content of up to 0.004 g/m3 and pre-absorbed hydrogen on the strength and ductility characteristics, short-term and long-term static crack resistance of 05Kh13N8M3 cast martensitic steel (in wt.%: 0.045 C, 0.38 Si, 12.9 Cr, 2.69 Mo, 0.43 Mn, 7.8 Ni, 0.057 La) at room temperature were studied. After hydrogen pre-charging for 4 h at a temperature of 773 K and a pressure of 5, 10, and 15 MPa, the hydrogen content of the specimens determined with a LECO TCH 600 device by infrared adsorption with melting was 3.3, 4.9, and 7.6 ppm, respectively. It was found that under short-term loading, the intensity of the effect of hydrogen on the fracture toughness of steel increases with an increase in the absorbed hydrogen content, crack sharpness, and a decrease in the loading rate. At the maximum hydrogen concentration of 7.6 ppm and a tensile rate of 0.1 mm/min, the relative elongation, lateral contraction ratio of smooth 25 mm long cylindrical specimens with a test portion diameter of 5 mm and the critical stress intensity factor of beam specimens measuring 20×10×100 mm with a relative length of the pre-induced crack of \(\upvarepsilon =\) 0.53 decrease almost twofold. At the same concentration, hydrogen does not affect the stress intensity factor of cracked specimens at a rate of 10 mm/min and specimens with a stress concentrator in the form of a notch with a tip radius of 0.065 mm at a rate of 0.1 mm/min. Under long-term static loading with a test duration of 300 h of double-cantilever beam specimens in the form of a rectangular plate 10 mm thick with milled grooves 3 mm deep and a tip angle of 60°, the threshold value of the stress intensity factor decreases. The rate of subcritical crack growth in the second portion of the hydrogen cracking diagram increases in proportion to the logarithm of hydrogen concentration.
期刊介绍:
Strength of Materials focuses on the strength of materials and structural components subjected to different types of force and thermal loadings, the limiting strength criteria of structures, and the theory of strength of structures. Consideration is given to actual operating conditions, problems of crack resistance and theories of failure, the theory of oscillations of real mechanical systems, and calculations of the stress-strain state of structural components.