利用 Averrhoa bilimbi(L)果实的水提取物进行生物还原,快速简便地根据 pH 值合成绿色氧化锌光催化剂

IF 0.7 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING International Journal of Materials Research Pub Date : 2023-12-14 DOI:10.1515/ijmr-2022-0433
Rajita Ramanarayanan, S. Swaminathan, Bhabhina Ninnora Meethal
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引用次数: 0

摘要

摘要 本研究报告了一种经济、环保的纳米氧化锌合成技术。在这种一锅合成方法中,使用了 Averrhoa bilimbi (L) 果实的水提取物来还原和稳定氧化锌纳米粒子。通过调节合成介质的 pH 值,获得了不同尺寸、形状和性质的合成纳米材料。利用 X 射线衍射技术、漫反射光谱、光致发光和扫描电子显微镜分析了植物化学物质封端的 ZnO 纳米粒子的特性。从扫描电子显微镜图像中观察到了随着 pH 值变化而发生的形态变化。在常温下合成时间短、产率高是该方法的显著特点。合成的氧化锌纳米粒子显示出卓越的光催化活性和超亲水性,可广泛应用于各种领域。
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Fast and facile pH tailored green synthesized ZnO photocatalyst by biogenic reduction using water extract of Averrhoa bilimbi (L) fruit
Abstract The present study reports an economical and environmentally friendly technique for the synthesis of zinc oxide nanoparticles. The water extract of Averrhoa bilimbi (L) fruit was used in this one-pot synthesis approach for ZnO nanoparticle reduction and stabilisation. Varied size, shape and properties of the synthesized nanomaterials were obtained by tuning the pH of the synthesis medium. X-ray diffraction techniques, diffuse reflectance spectroscopy, photoluminescence and scanning electron microscopy analysis were used for characterizing phytochemical capped ZnO nanoparticles. The morphological change with varying pH was observed from scanning electron microscopy images. Short duration of synthesis with high yield product at ambient room temperature are the salient features of this procedure. The synthesised ZnO nanoparticles showed excellent photocatalytic activity and superhydrophilicity to be used in a wide range of applications.
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来源期刊
CiteScore
1.30
自引率
12.50%
发文量
119
审稿时长
6.4 months
期刊介绍: The International Journal of Materials Research (IJMR) publishes original high quality experimental and theoretical papers and reviews on basic and applied research in the field of materials science and engineering, with focus on synthesis, processing, constitution, and properties of all classes of materials. Particular emphasis is placed on microstructural design, phase relations, computational thermodynamics, and kinetics at the nano to macro scale. Contributions may also focus on progress in advanced characterization techniques. All articles are subject to thorough, independent peer review.
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