使用基于壳聚糖的水凝胶复合材料去除三聚氰胺红

H. Sebti, Nihel Dib, F. Z. Sebba, B. Bounaceur
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引用次数: 0

摘要

本研究利用(N,N'亚甲基双丙烯酰胺)MBAm 作为交联剂,过硫酸钾(PPS)作为引发剂,对(2-丙烯酰胺基-2-甲基-1-丙烷磺酸)AMPS 进行自由基共聚合合成,以生产壳聚糖基复合水凝胶。研究涉及不同质量的壳聚糖(250、500 和 1000 毫克)。使用傅立叶变换红外光谱(FTIR)、热重分析(TGA)、扫描电镜(SEM)、紫外可见光(UV-visible)和 STEM 技术对获得的复合材料和染料吸附过程进行了表征。对蒸馏水中的溶胀特性进行了研究,结果表明聚(AMPS-g-MBAm)/壳聚糖水凝胶(1000 毫克)在 25°C 和 37°C 温度下的溶胀率超过了聚(AMPS-g-MBAm)/壳聚糖水凝胶(250 毫克和 500 毫克)。此外,还对染料的吸附能力进行了研究,结果表明聚(AMPS-g-MBAm)/壳聚糖(1000 毫克)在不同温度下的吸附能力超过了聚(AMPS-g-MBAm)/壳聚糖(250 毫克和 500 毫克)。
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Removal of trisacryl red using hydrogels composites based on chitosan
This study entails the radical copolymerization synthesis of (2-acrylamido-2-methyl-1-propane sulfonic acid) AMPS, utilizing (N,N’methylene bis-acrylamide) MBAm as a cross-linking agent and potassium persulfate (PPS) as an initiator to produce chitosan-based composite hydrogels. The investigation involved the various masses of chitosan (250, 500, and 1000 mg). The characterization of the obtained composites and the dye adsorption process was carried out using FTIR, TGA, SEM, UV-visible, and STEM techniques. Swelling properties in distilled water were examined, revealing that the swelling rates at temperatures of 25°C and 37°C for the hydrogel of poly(AMPS-g-MBAm)/chitosan (1000 mg) exceed those of hydrogels with poly(AMPS-g-MBAm)/chitosan (250 and 500 mg). Furthermore, the sorption capacities of the dye were investigated, demonstrating that the sorption capacities of poly (AMPS-g-MBAm)/chitosan (1000 mg) at different temperatures surpass those of poly(AMPS-g-MBAm)/chitosan (250mg, and 500 mg).
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来源期刊
Communications in Science and Technology
Communications in Science and Technology Engineering-Engineering (all)
CiteScore
3.20
自引率
0.00%
发文量
13
审稿时长
24 weeks
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