{"title":"使用基于壳聚糖的水凝胶复合材料去除三聚氰胺红","authors":"H. Sebti, Nihel Dib, F. Z. Sebba, B. Bounaceur","doi":"10.21924/cst.8.2.2023.1278","DOIUrl":null,"url":null,"abstract":"This study entails the radical copolymerization synthesis of (2-acrylamido-2-methyl-1-propane sulfonic acid) AMPS, utilizing (N,N’methylene bis-acrylamide) MBAm as a cross-linking agent and potassium persulfate (PPS) as an initiator to produce chitosan-based composite hydrogels. The investigation involved the various masses of chitosan (250, 500, and 1000 mg). The characterization of the obtained composites and the dye adsorption process was carried out using FTIR, TGA, SEM, UV-visible, and STEM techniques. Swelling properties in distilled water were examined, revealing that the swelling rates at temperatures of 25°C and 37°C for the hydrogel of poly(AMPS-g-MBAm)/chitosan (1000 mg) exceed those of hydrogels with poly(AMPS-g-MBAm)/chitosan (250 and 500 mg). Furthermore, the sorption capacities of the dye were investigated, demonstrating that the sorption capacities of poly (AMPS-g-MBAm)/chitosan (1000 mg) at different temperatures surpass those of poly(AMPS-g-MBAm)/chitosan (250mg, and 500 mg).","PeriodicalId":36437,"journal":{"name":"Communications in Science and Technology","volume":" 580","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Removal of trisacryl red using hydrogels composites based on chitosan\",\"authors\":\"H. Sebti, Nihel Dib, F. Z. Sebba, B. Bounaceur\",\"doi\":\"10.21924/cst.8.2.2023.1278\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study entails the radical copolymerization synthesis of (2-acrylamido-2-methyl-1-propane sulfonic acid) AMPS, utilizing (N,N’methylene bis-acrylamide) MBAm as a cross-linking agent and potassium persulfate (PPS) as an initiator to produce chitosan-based composite hydrogels. The investigation involved the various masses of chitosan (250, 500, and 1000 mg). The characterization of the obtained composites and the dye adsorption process was carried out using FTIR, TGA, SEM, UV-visible, and STEM techniques. Swelling properties in distilled water were examined, revealing that the swelling rates at temperatures of 25°C and 37°C for the hydrogel of poly(AMPS-g-MBAm)/chitosan (1000 mg) exceed those of hydrogels with poly(AMPS-g-MBAm)/chitosan (250 and 500 mg). Furthermore, the sorption capacities of the dye were investigated, demonstrating that the sorption capacities of poly (AMPS-g-MBAm)/chitosan (1000 mg) at different temperatures surpass those of poly(AMPS-g-MBAm)/chitosan (250mg, and 500 mg).\",\"PeriodicalId\":36437,\"journal\":{\"name\":\"Communications in Science and Technology\",\"volume\":\" 580\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-12-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Communications in Science and Technology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.21924/cst.8.2.2023.1278\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Engineering\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Communications in Science and Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21924/cst.8.2.2023.1278","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Engineering","Score":null,"Total":0}
Removal of trisacryl red using hydrogels composites based on chitosan
This study entails the radical copolymerization synthesis of (2-acrylamido-2-methyl-1-propane sulfonic acid) AMPS, utilizing (N,N’methylene bis-acrylamide) MBAm as a cross-linking agent and potassium persulfate (PPS) as an initiator to produce chitosan-based composite hydrogels. The investigation involved the various masses of chitosan (250, 500, and 1000 mg). The characterization of the obtained composites and the dye adsorption process was carried out using FTIR, TGA, SEM, UV-visible, and STEM techniques. Swelling properties in distilled water were examined, revealing that the swelling rates at temperatures of 25°C and 37°C for the hydrogel of poly(AMPS-g-MBAm)/chitosan (1000 mg) exceed those of hydrogels with poly(AMPS-g-MBAm)/chitosan (250 and 500 mg). Furthermore, the sorption capacities of the dye were investigated, demonstrating that the sorption capacities of poly (AMPS-g-MBAm)/chitosan (1000 mg) at different temperatures surpass those of poly(AMPS-g-MBAm)/chitosan (250mg, and 500 mg).