研究通过水热法制备并与动植物提取物(洋葱皮和壳聚糖皮)混合的二氧化钛纳米粒子的抗菌活性

Falah Ali, Muslim A. Abid, Wisam J. Aziz
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摘要

二氧化钛纳米粒子 TiO2 的初步生产采用了水热法。洋葱皮和壳聚糖皮提取物采用生物合成方法制成。利用(紫外-可见光)特性,研究了 TiO2 和 TiO2 与洋葱皮和壳聚糖皮提取物的结构特征,发现 TiO2 NPs、TiO2 + 洋葱皮和 TiO2 + 壳聚糖皮的吸收边缘分别在 236 nm、244 nm 和 237.5 nm 左右。根据 X 射线衍射(XRD)研究,TiO2 的一些峰的形态表明其为四方金红石相。对 TiO2 NPs、TiO2 + 洋葱皮和 TiO2 + 壳聚糖皮进行了能量色散 X 射线(EDX)分析。场发射扫描电子显微镜(FE-SEM)显示,TiO2 NPs、TiO2 + 洋葱皮和 TiO2 + 壳聚糖皮的直径范围分别为(43.32 nm 至 47.77 nm)、(34.11 nm 至 62.77 nm)和(32.22 nm 至 35.11 nm)。研究了 TiO2 和 TiO2 与提取物纳米粒子对细菌生长的影响,观察到 TiO2 和 TiO2 与提取物纳米粒子对细菌生长的影响存在差异。
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Examination the antibacterial activity for the TiO2 nanoparticles which is prepared by hydrothermal method and mixed with plant and animal extracts (Onion peels and Chitosan peels)
Initial production of the titanium dioxide nanoparticles TiO2 used the hydrothermal process. The onion peels and chitosan peel extracts, which are made using the Bio-synthesize approach. By using (UV-Vis) properties, the structural characteristics of TiO2 and TiO2 with extract from onion peels and chitosan peels were studied, and find the absorption edge of TiO2 NPs, TiO2 + onion peels and TiO2 + chitosan peels is around 236 nm, 244 nm and 237.5 nm respectively. The pattern of TiO2 for a number of peaks suggested a tetragonal rutile phase, according to X-ray diffraction (XRD) research. Energy dispersive X-ray, (EDX) was done for TiO2 NPs, TiO2 + onion peels and TiO2 + chitosan peels. Field emission scanning electron microscopy (FE-SEM) shows that the diameters ranging of TiO2 NPs, TiO2 + onion peels and TiO2 + chitosan peels from (43.32 nm to 47.77 nm), (34.11 nm to 62.77 nm) and (32.22 nm to 35.11 nm) respectively. Studying was done on the effect of TiO2 & TiO2 with extracts nanoparticles on bacterial growth, a variation was observed in the effect of the TiO2 & TiO2 with extracts on the growth of bacteria.
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