基于 ICP-MS 的喂食昆虫 Tenebrio molitor 重金属分析新方法

Ravisankar M., Alexandar S., S. R, Kumar M., Venkateswarlu B. S.
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引用次数: 0

摘要

饲养昆虫体内的重金属积累正成为一个主要的食品安全问题,因为它会通过有毒化合物进入人类食物链而威胁人类健康。为利用 ICP-MS 测定褐飞虱饲养昆虫体内的重金属,本研究设计并验证了一种准确、灵敏的方法。新方法的标准,如线性和范围、准确度、精密度、选择性、检出限和定量限等,都被用来验证这种方法。目前的技术具有线性关系,相关系数不小于 0.99。所开发的方法的准确度为 91.13%至 104.93%。当金属在规格水平上的重复响应 RSD 小于 20% 时,该方法也是精确的。由于某些金属的检出限和定量限较低,因此该方法可以检测和定量低浓度的金属。
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A New ICP-MS Based Approach for the Analysis of Heavy Metals in Feeder Insect Tenebrio molitor
Heavy metal accumulation in feeder insects is becoming a major food safety concern as it is a threat to human health through the transmission of toxic compounds into the human food chain. For the determination of heavy metals in Tenebrio molitor feeder insect by ICP-MS, an accurate and sensitive approach has been devised and validated in this study. The criteria for new methods, such as linearity and range, accuracy, precision, selectivity, limit of detection, and limit of quantitation are used to verify this method. The current technique exhibits linearity with correlation coefficient values not less than 0.99. The developed method shows accuracy ranging from 91.13 to 104.93%. When the RSD of the responses of replicates of the metals at specification levels is less than 20%, the approach is also precise. This method enables the detection and quantification of certain metals at low concentrations due to their low limit of detection and limit of quantification.
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