{"title":"黄瓜(Cucumis sativus L.)上乙氰菊酯和吡虫啉复配产品的残留行为和消费者风险评估","authors":"Sakshi Sharma, Jatiender Kumar Dubey, Sapna Katna, Ajay Sharma, Deepika Shandil, Pankaj Sharma, Nisha Devi, Arvind Kumar, Shubhra Singh, Nimisha Thakur","doi":"10.1007/s00769-024-01573-2","DOIUrl":null,"url":null,"abstract":"<div><p>Residue behavior and consumer risk assessment of combination of betacyfluthrin and imidacloprid at recommended dose (X) and double the recommended dose (2X) on cucumber crop were studied during <i>kharif</i> season, 2019. The combination product was applied thrice as foliar sprays at 7 days interval with first application at fruit initiation stage. Residues of betacyfluthrin and imidacloprid were detected using gas chromatography-electron capture detector and high pressure liquid chromatography, respectively, after the extraction and clean-up of samples with modified QuEChERS technique. The average initial deposits at X and 2X dose of betacyfluthrin were 0.69 and 1.41 mg kg<sup>−1</sup>, which dissipated to half of its concentration in 1.51 and 1.73 days with a suggested safe waiting period of 5.73 and 8.34 days whereas, for imidacloprid, initial deposits were 0.84 and 1.56 mg kg<sup>−1</sup>, which dissipated to half of its concentration in 1.29 and 1.51 days with a suggested safe waiting period of 5.24 and 7.49 days, respectively. Residues in soil samples collected at harvest were found to be below determination level for both components. Dietary risk assessment calculated as hazard quotient came out to be less than 1, thus establishing the safety of combination product of betacyfluthrin and imidacloprid for consumers when used following good agricultural practices.</p></div>","PeriodicalId":454,"journal":{"name":"Accreditation and Quality Assurance","volume":"29 2","pages":"141 - 151"},"PeriodicalIF":0.8000,"publicationDate":"2024-02-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Residue behavior and consumer risk assessment of combination product of betacyfluthrin and imidacloprid on cucumber (Cucumis sativus L.)\",\"authors\":\"Sakshi Sharma, Jatiender Kumar Dubey, Sapna Katna, Ajay Sharma, Deepika Shandil, Pankaj Sharma, Nisha Devi, Arvind Kumar, Shubhra Singh, Nimisha Thakur\",\"doi\":\"10.1007/s00769-024-01573-2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Residue behavior and consumer risk assessment of combination of betacyfluthrin and imidacloprid at recommended dose (X) and double the recommended dose (2X) on cucumber crop were studied during <i>kharif</i> season, 2019. The combination product was applied thrice as foliar sprays at 7 days interval with first application at fruit initiation stage. Residues of betacyfluthrin and imidacloprid were detected using gas chromatography-electron capture detector and high pressure liquid chromatography, respectively, after the extraction and clean-up of samples with modified QuEChERS technique. The average initial deposits at X and 2X dose of betacyfluthrin were 0.69 and 1.41 mg kg<sup>−1</sup>, which dissipated to half of its concentration in 1.51 and 1.73 days with a suggested safe waiting period of 5.73 and 8.34 days whereas, for imidacloprid, initial deposits were 0.84 and 1.56 mg kg<sup>−1</sup>, which dissipated to half of its concentration in 1.29 and 1.51 days with a suggested safe waiting period of 5.24 and 7.49 days, respectively. Residues in soil samples collected at harvest were found to be below determination level for both components. Dietary risk assessment calculated as hazard quotient came out to be less than 1, thus establishing the safety of combination product of betacyfluthrin and imidacloprid for consumers when used following good agricultural practices.</p></div>\",\"PeriodicalId\":454,\"journal\":{\"name\":\"Accreditation and Quality Assurance\",\"volume\":\"29 2\",\"pages\":\"141 - 151\"},\"PeriodicalIF\":0.8000,\"publicationDate\":\"2024-02-02\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Accreditation and Quality Assurance\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s00769-024-01573-2\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, ANALYTICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Accreditation and Quality Assurance","FirstCategoryId":"5","ListUrlMain":"https://link.springer.com/article/10.1007/s00769-024-01573-2","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, ANALYTICAL","Score":null,"Total":0}
Residue behavior and consumer risk assessment of combination product of betacyfluthrin and imidacloprid on cucumber (Cucumis sativus L.)
Residue behavior and consumer risk assessment of combination of betacyfluthrin and imidacloprid at recommended dose (X) and double the recommended dose (2X) on cucumber crop were studied during kharif season, 2019. The combination product was applied thrice as foliar sprays at 7 days interval with first application at fruit initiation stage. Residues of betacyfluthrin and imidacloprid were detected using gas chromatography-electron capture detector and high pressure liquid chromatography, respectively, after the extraction and clean-up of samples with modified QuEChERS technique. The average initial deposits at X and 2X dose of betacyfluthrin were 0.69 and 1.41 mg kg−1, which dissipated to half of its concentration in 1.51 and 1.73 days with a suggested safe waiting period of 5.73 and 8.34 days whereas, for imidacloprid, initial deposits were 0.84 and 1.56 mg kg−1, which dissipated to half of its concentration in 1.29 and 1.51 days with a suggested safe waiting period of 5.24 and 7.49 days, respectively. Residues in soil samples collected at harvest were found to be below determination level for both components. Dietary risk assessment calculated as hazard quotient came out to be less than 1, thus establishing the safety of combination product of betacyfluthrin and imidacloprid for consumers when used following good agricultural practices.
期刊介绍:
Accreditation and Quality Assurance has established itself as the leading information and discussion forum for all aspects relevant to quality, transparency and reliability of measurement results in chemical and biological sciences. The journal serves the information needs of researchers, practitioners and decision makers dealing with quality assurance and quality management, including the development and application of metrological principles and concepts such as traceability or measurement uncertainty in the following fields: environment, nutrition, consumer protection, geology, metallurgy, pharmacy, forensics, clinical chemistry and laboratory medicine, and microbiology.