微弧氧化后 AZ31 镁合金上的环氧树脂/多壁碳纳米管导电涂层研究

C. Zhang, C. Wang, B. Jiang, R. Song
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引用次数: 0

摘要

经过微弧氧化处理后,AZ31 镁合金的表面性能得到了改善。然而,微弧氧化处理会导致高绝缘,从而限制了其在电子设备中的应用。为了提高导电性,研究人员在环氧树脂中添加了多壁碳纳米管(MWCNTs),从而开发出一种导电涂层。通过扫描电镜、热重分析仪、四探针电导率仪、高温摩擦磨损测试仪和电化学工作站对涂层的微观结构和性能进行了测试。结果表明,当 MWCNT 含量为 4[式中:见正文]wt%时,可获得最佳导电性,电阻率为 303[式中:见正文][式中:见正文]m。此外,MWCNT 被填充到环氧树脂的网络结构中,从而增加了涂层的密度,提高了其耐磨性和耐腐蚀性。
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STUDY ON EPOXY RESIN/MULTI-WALLED CARBON NANOTUBES CONDUCTIVE COATING ON AZ31 MAGNESIUM ALLOY AFTER MICRO-ARC OXIDATION
After micro-arc oxidation, the surface properties of AZ31 magnesium alloy have been improved. However, micro-arc oxidation treatment leads to high insulation, which limits its application in electronic devices. To increase conductivity, a conductive coating was developed by adding multi-walled carbon nanotubes (MWCNTs) to the epoxy resin. The microstructure and performance of the coating were tested by SEM, thermogravimetric analyzer, four-probe conductivity meter, high-temperature friction and wear tester, and electrochemical workstation. The results indicate that the optimal conductivity with a resistivity of 303[Formula: see text][Formula: see text]m is obtained when the MWCNT content is at 4[Formula: see text]wt%. In addition, MWCNTs are filled with a network structure of epoxy resin, which increases the density of the coating and enhances their wear and corrosion resistance.
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