内部碳化导致砂浆自愈合时裂缝起源的声发射波形表征

Wenting Li, Shan Qiang, Qi Wei
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引用次数: 0

摘要

在这项研究中,通过可溶性 Na2CO3 和 Ca(OH)2 的 "内置 "碳化实现了砂浆的自愈合。通过用 Ca(OH)2 和 Na2CO3 溶液调节试样,研究了内部或外部碳酸根离子和钙离子对裂缝中方解石形成的影响。在愈合前后的加载过程中,对声学事件进行了监测和比较。此外,还进行了校准测试,以区分基体断裂和愈合产物的特征声发射事件。结果发现,声能与 FMA(最大振幅时的频率)的分布以及命中与持续时间的分布呈现出与校准一致的趋势。重装过程中拉伸与剪切裂纹比率的变化说明了裂纹的自愈合效应。同时,X 射线衍射分析表明,自愈合试样的裂缝中形成了更多的方解石。与其他试样相比,经过预处理的含方解石试样由于内部有 CO32- 和足够的 Ca2+,因此表现出了主要的自愈合效应。
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Acoustic Emission Waveform Characterization of Crack Origin In Self-Healing of Mortar Due to Internal Carbonation
In this study, self-healing of mortar was achieved by “built-in” carbonation of soluble Na2CO3 and Ca(OH)2. The effect of carbonate and calcium ions, available either internally or externally by conditioning the specimens with Ca(OH)2 and Na2CO3 solution, on the formation of calcite in cracks was investigated. The acoustic events were monitored and compared in the loading process before and after healing. Furthermore, a calibration test was carried out to distinguish the characteristic acoustic emission events of the fracture of the matrix and of healing products. It was found that the distribution of acoustic energy with FMA (frequency at maximum amplitude) and the hits with duration show a consistent trend with that of calibration. The change of tensile to shear cracking ratio in reloading illustrates a self-healing effect of cracks. Meanwhile, X-ray diffraction analysis indicates more calcite formed in the crack of self-healing specimens. The pretreated ceramsite-containing specimens exhibit the predominate self-healing effect due to the internally available CO32– and sufficient Ca2+ as compared to the others.
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