溶剂微萃取的进展:当代的最新发展和多样化应用

Priyanka Rani, Bibhu Prasad Nanda, R. Narang, Rohit Bhatia
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摘要

溶剂微萃取(SME)旨在选择性地分离出所需的分析物,同时尽量减少萃取样品中干扰物质的存在。单滴微萃取(SDME)可以通过不同的方法与各种分析方法相结合,以增强其功能并改进对萃取化合物的分析,如气相色谱和液相色谱法可以提高灵敏度、选择性和检测复杂基质中痕量分析物的能力。综述重点介绍了固相微萃取的复杂性,并阐明了其操作原理。此外,它还探讨了各种类型的固相微萃取器,详细介绍了它们各自的优点、缺点以及在未来的潜在应用。文中还对中空纤维-液相微萃取的构造和工作原理及其类型进行了典型解释。还讨论了中小型企业在医疗和生物医学领域的应用,从食品分析到环境分析,如水的分析和净化、有机污染物、药物分析和新药筛选,并以表格形式进行了说明。两种分析技术的优缺点都以表格的形式给出,不同类型的先进 SME 技术之间的广泛比较也为环境监测、食品安全和提炼水样中的杂质提供了新的方向。综述以适当的方式全面概述了中小型企业的当前进展、近期障碍和未来可能性。尽管取得了许多令人鼓舞的进展,但中小型企业的利用仍然是一个充满挑战的领域。
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Advancements in solvent microextraction: Recent developments and diverse applications in the modern era
Solvent microextraction (SME) is designed to selectively isolate desired analytes while minimizing the presence of interfering substances in the extracted sample. There are different approaches from which single‐drop microextraction (SDME) can be amalgamated with various analytical methods to enhance its functionalities and improve the analysis of extracted compounds like gas chromatography, and liquid chromatography amplify sensitivity, selectivity, and the capacity to detect trace amounts of analytes in complex matrices. The review focuses on the intricacies of solid‐phase microextraction and elucidates its operational principles. Additionally, it explores various types of SDMEs, detailing their respective benefits, drawbacks, and potential applications in the future. A typical explanation of the construction and working of hollow fiber‐liquid phase microextraction as well as its types has been discussed. The applications of SMEs in the medical and biomedical fields from food analysis to environmental analysis like analysis and purification of water, organic pollutants, drug analysis, and screening of new drugs have been discussed and also illustrated in tabular form. The pros and cons of both analytical techniques are given in a tabular manner as well a broad comparison between different types of advanced SME techniques provides a new direction for environmental monitoring, food safety, and refining of impurities from water samples. The review provides a comprehensive overview of the current progress, recent obstacles, and future possibilities of SMEs in an appropriate manner. Despite numerous promising advancements, the utilization of SMEs remains a challenging field.
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