利用茶树和芒果叶提取物制备纳米氧化锌,用于亚甲基蓝的光催化剂

S. W. Suciyati, Junaidi Junaidi, R. Situmeang, Posman Manurung
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引用次数: 0

摘要

本研究旨在利用茶叶(Cnidoscolus aconitifolius)和芒果叶提取物(Mangifera indica)合成纳米氧化锌,作为环境友好型光催化剂。纳米氧化锌采用绿色合成法合成,树叶提取物作为还原剂和纳米颗粒尺寸稳定剂。样品采用两种方法制备,即纳米 ZnO-1 和纳米 ZnO-2。傅立叶变换红外光谱(FTIR)分析结果表明,代谢物化合物在纳米氧化锌合成中起到了重要作用。X 射线衍射(XRD)和透射电子显微镜(TEM)显示晶体尺寸在纳米范围内,并观察到球形纳米棒形态。紫外-可见光漫反射光谱(UV-Vis DRS)测定其带隙能分别为 2.97 eV 和 3.17 eV。此外,光催化活性测试表明,90 分钟后的光催化剂性能为 68.86%(纳米 ZnO-1)和 96.46%(纳米 ZnO-2)。
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Nano-ZnO prepared by using chaya and mango leaves extract for photocatalyst of methylene blue
This research aimed to synthesize nano-ZnO from chaya (Cnidoscolus aconitifolius) and mango leaves extract (Mangifera indica) as environmentally friendly photocatalysts. Nano-ZnO was synthesized using green synthesis, with leaves extracts as reducing agents and nanoparticle size stabilizers. The samples were prepared using two methods, namely nano-ZnO-1 and nano-ZnO-2. The results of Fourier transform infrared spectroscopy (FTIR) analysis showed the contribution of metabolite compounds in nano-ZnO synthesis. X-ray diffraction (XRD) and transmission electron microscopy (TEM) showed the crystal size in nano range, with spherical nanorod morphology observed. Ultraviolet-visible diffuse reflectance spectroscopy (UV-Vis DRS) determined the band gap energy of 2.97 eV and 3.17 eV. Furthermore, photocatalytic activity test showed that photocatalyst performance after 90 min was 68.86% (nano-ZnO-1) and 96.46% (nano-ZnO-2).
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