人工老化纤维增强复合材料的粘接强度。(体外研究)

Zeinab Ahmed, Sarah Abdel Moniem, O. Ghallab
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摘要

目的:本研究旨在探讨时间和表面处理对修复纤维增强复合材料与纳米混合复合材料剪切粘接强度的影响。材料和方法:制备了 80 个 Ever-X Posterior(欧洲 GC 公司)试样。根据修复时间(24 小时后和一个月后)将其平均分为两组。然后,每组又根据表面处理分为五个小组(1-无表面处理;2-金刚石涂层毛刺、两步自刻粘合剂;3-金刚石涂层毛刺、两步自刻粘合剂、硅烷;4-空气研磨、两步自刻粘合剂;5-空气研磨、两步自刻粘合剂、硅烷)。在修复材料中加入纳米杂化复合材料,厚度为 2 毫米。所有组均进行了 5000 次热循环。采用双向方差分析对数据进行统计分析。结果:表面处理和修复时间都对修复复合材料的 SBS 有显著影响。在一个月后进行修复的子组(空气磨蚀和粘接剂)中,修复效果最好。结论一个月的复发对 FRC 材料的修复强度没有明显影响。气磨被认为是一种强有力的机械表面处理方法,可使 FRC 材料获得非常显著的修复强度。
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Bond Strength of Artificially Aged Fiber Reinforced Composite Material. (An in-vitro study)
Aim: The aim of this study was to investigate the effect of time and surface treatments on shear bond strength of repaired fiber reinforced composite to nano-hybrid composite material. Materials and methods: Eighty specimens were prepared of ever-X Posterior (GC Europe). They were equally divided into two groups according to time of repair (after 24 hours and one month). Then, each group subdivided to five subgroups according to surface treatment (1-No surface treatment, 2-Diamond coated bur, two step self-etch adhesive, 3-Diamond coated bur, two step self-etch adhesive, silane, 4-Air abrasion, two step self-etch adhesive, 5-Air abrasion, two step self-etch adhesive, silane). A nano-hybrid composite was added as a material of repair in 2 mm thickness. All groups were thermocycled for 5000 cycles. The two-way ANOVA test was employed for statistical analysis of the data. Results: both the surface treatments and the time of repair had significant effect on SBS of repaired composite. The highest results were achieved in subgroup (Air abrasion and bonding agent) when repaired after one month. Conclusion: One month time relapse has no drastic effect on repair strength of FRC material. Air abrasion is considered a powerful mechanical surface treatment for achieving a highly significant repair strength of FRC material.
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