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引用次数: 0
摘要
本研究通过无电解电镀和表面改性,有效地在 AZ91 镁合金上镀上了超疏水的 Ni-B/ 氧化石墨烯(GO)涂层。采用扫描电子显微镜、能量色散谱、X 射线粉末衍射和 X 射线光电子能谱分析来描述 Ni-B/GO 涂层的发展过程。结果表明,超疏水涂层的微纳米粗糙结构是由于 GO 和十二烷基硫酸钠的协同作用及其各自对涂层的影响。研究还发现,纳米级的 GO 粒子包裹着未充分发育的镍晶粒。同时,典型的超疏水涂层横截面的组成和结构显示了粗糙结构的生长。此外,水接触角高达 161.6° 的超疏水涂层具有无定形结构。因此,微纳米涂层为制备镁合金超疏水涂层提供了一个新的视角。
A new approach for constructing rough structures to fabricate superhydrophobic Ni–B/graphene oxide (GO) coating
In this study, AZ91 magnesium alloy was effectively coated with a superhydrophobic Ni–B/graphene oxide (GO) coating via electroless plating and surface modification. Scanning electron microscopy, energy dispersion spectrum, X-ray powder diffraction, and X-ray photoelectron spectroscopy analysis were employed to describe the development of Ni–B/GO coatings. The results show that the micro–nano rough structures of the superhydrophobic coating were owing to the synergistic action of GO and sodium dodecyl sulphate and their respective effects on the coating. It was also found that the nanoscale GO particle wrapped around the underdeveloped nickel grains. Also, the composition and structure of the typical superhydrophobic coating cross-section revealed the growth of the rough structures. Furthermore, the superhydrophobic coating with a water contact angle of up to 161.6° had an amorphous structure. The micro–nano coating therefore provides a novel viewpoint for preparing superhydrophobic coating on magnesium alloy.
期刊介绍:
Surface Engineering provides a forum for the publication of refereed material on both the theory and practice of this important enabling technology, embracing science, technology and engineering. Coverage includes design, surface modification technologies and process control, and the characterisation and properties of the final system or component, including quality control and non-destructive examination.