通过添加废玻璃粉低温烧结多孔沸石球体

Ayse Kurt, A. Kalemtas
{"title":"通过添加废玻璃粉低温烧结多孔沸石球体","authors":"Ayse Kurt, A. Kalemtas","doi":"10.13005/msri/200302","DOIUrl":null,"url":null,"abstract":"ABSTRACT: In this study, porous zeolite spheres were produced at a low temperature by a facile and economical method, sol-gel, using a natural zeolite from the Gördes region of Türkiye and waste soda glass powder. Waste glass powder was achieved by milling the recyclable waste soda glass bottles to be used as a source of silica. Elemental analysis of the waste glass was carried out by using X-ray fluorescence spectrometry. It was determined that Si (57.3 wt. %), Ca (20.9 wt. %), Na (13.9 wt. %), Mg (2.64 wt. %), and Al (1.64 wt. %) were the major constituents of the waste glass. Three different sphere compositions were designed containing 1:1, 3:2, and 7:3 zeolite:waste glass ratio. When the zeolite:waste glass ratio was 1:1 oval-shaped green spheres were achieved. For the compositions containing 3:2, and 7:3 zeolite:waste glass ratio spherical green samples were achieved. Prepared spheres were sintered at 300°, 400°, and 500°C for 1 h. It was observed that the samples could not maintain their spherical form when the sintering temperature was lower than 500°C. Scanning electron microscopy investigation of the spheres sintered at 500°C revealed that highly porous zeolite spheres, containing pores from ~20 µm to nanometre sizes, were achieved. Image J software was used to determine effect of composition on the size and size distribution of the sintered spheres.","PeriodicalId":18247,"journal":{"name":"Material Science Research India","volume":"57 3","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2024-01-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Low Temperature Sintering of Porous Zeolite Spheres via Waste Glass Powder Addition\",\"authors\":\"Ayse Kurt, A. Kalemtas\",\"doi\":\"10.13005/msri/200302\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ABSTRACT: In this study, porous zeolite spheres were produced at a low temperature by a facile and economical method, sol-gel, using a natural zeolite from the Gördes region of Türkiye and waste soda glass powder. Waste glass powder was achieved by milling the recyclable waste soda glass bottles to be used as a source of silica. Elemental analysis of the waste glass was carried out by using X-ray fluorescence spectrometry. It was determined that Si (57.3 wt. %), Ca (20.9 wt. %), Na (13.9 wt. %), Mg (2.64 wt. %), and Al (1.64 wt. %) were the major constituents of the waste glass. Three different sphere compositions were designed containing 1:1, 3:2, and 7:3 zeolite:waste glass ratio. When the zeolite:waste glass ratio was 1:1 oval-shaped green spheres were achieved. For the compositions containing 3:2, and 7:3 zeolite:waste glass ratio spherical green samples were achieved. Prepared spheres were sintered at 300°, 400°, and 500°C for 1 h. It was observed that the samples could not maintain their spherical form when the sintering temperature was lower than 500°C. Scanning electron microscopy investigation of the spheres sintered at 500°C revealed that highly porous zeolite spheres, containing pores from ~20 µm to nanometre sizes, were achieved. Image J software was used to determine effect of composition on the size and size distribution of the sintered spheres.\",\"PeriodicalId\":18247,\"journal\":{\"name\":\"Material Science Research India\",\"volume\":\"57 3\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2024-01-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Material Science Research India\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.13005/msri/200302\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Material Science Research India","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.13005/msri/200302","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

摘要:在这项研究中,使用来自土耳其戈尔杰斯地区的天然沸石和废苏打玻璃粉,通过溶胶-凝胶法在低温下生产出了多孔沸石球。废玻璃粉是通过研磨可回收的废苏打玻璃瓶作为二氧化硅来源而获得的。利用 X 射线荧光光谱法对废玻璃进行了元素分析。结果表明,废玻璃的主要成分是硅(57.3 wt.%)、钙(20.9 wt.%)、纳(13.9 wt.%)、镁(2.64 wt.%)和铝(1.64 wt.%)。设计了三种不同的球体成分,沸石与废玻璃的比例分别为 1:1、3:2 和 7:3。当沸石与废玻璃的比例为 1:1 时,可得到椭圆形的绿色球体。当沸石与废玻璃的比例为 3:2 和 7:3 时,可制得球形绿色样品。将制备好的球体在 300°、400° 和 500°C 温度下烧结 1 小时后发现,当烧结温度低于 500°C 时,样品无法保持球形。对 500°C 烧结的球体进行的扫描电子显微镜研究表明,烧结出的沸石球体具有高孔隙率,孔隙大小从 ~20 微米到纳米不等。使用 Image J 软件确定了成分对烧结球的尺寸和尺寸分布的影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Low Temperature Sintering of Porous Zeolite Spheres via Waste Glass Powder Addition
ABSTRACT: In this study, porous zeolite spheres were produced at a low temperature by a facile and economical method, sol-gel, using a natural zeolite from the Gördes region of Türkiye and waste soda glass powder. Waste glass powder was achieved by milling the recyclable waste soda glass bottles to be used as a source of silica. Elemental analysis of the waste glass was carried out by using X-ray fluorescence spectrometry. It was determined that Si (57.3 wt. %), Ca (20.9 wt. %), Na (13.9 wt. %), Mg (2.64 wt. %), and Al (1.64 wt. %) were the major constituents of the waste glass. Three different sphere compositions were designed containing 1:1, 3:2, and 7:3 zeolite:waste glass ratio. When the zeolite:waste glass ratio was 1:1 oval-shaped green spheres were achieved. For the compositions containing 3:2, and 7:3 zeolite:waste glass ratio spherical green samples were achieved. Prepared spheres were sintered at 300°, 400°, and 500°C for 1 h. It was observed that the samples could not maintain their spherical form when the sintering temperature was lower than 500°C. Scanning electron microscopy investigation of the spheres sintered at 500°C revealed that highly porous zeolite spheres, containing pores from ~20 µm to nanometre sizes, were achieved. Image J software was used to determine effect of composition on the size and size distribution of the sintered spheres.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Utilizing a Variable Material Approach to Combat Climate Change Enhancing Sustainable Concrete Investigating the Feasibility of POND ASH as a Partial Replacement for Fine Aggregate in GGBS-Based Optimizing Concrete Strength with the Partial Replacement of Aggregate with Ceramic Tiles for Sustainable Construction Low Temperature Sintering of Porous Zeolite Spheres via Waste Glass Powder Addition Ultrasonic-Assisted Synthesis of Silicon/Exfoliated-Graphite Nanocomposite as Anode Material for Lithium-Ion Batteries
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1