Nb2O5 和 B2O3 对溶胶-凝胶法制备的 TiO2 纳米氧化物光催化和抗菌活性的影响

A. Bachvarova-Nedelcheva, R. Iordanova, Nelly Georgieva, Veronica Nemska, Tsvetelina Foteva, A. Stoyanova
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引用次数: 0

摘要

通过水溶胶凝胶法获得了含有 B2O3 和 Nb2O5 的二氧化钛粉末。制备的凝胶在 200°C - 500°C 的温度范围内分步加热,随后通过 XRD、IR 和 UV-Vis 分析进行表征。TiO2(锐钛型)是单晶相,其检测温度高达 500°C。光催化测试表明,所研究的样品对孔雀石绿有机染料具有光催化活性,TiO2/Nb2O5 的光催化活性高于 TiO2/B2O3 样品。这些组合物对大肠杆菌 NBIMCC K12 407 和枯草杆菌 NBIMCC 3562 具有良好的抗菌活性。
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INFLUENCE OF Nb2O5 AND B2O3 ON THE PHOTOCATALYTIC AND ANTIBACTERIAL ACTIVITY OF SOL-GEL DERIVED TiO2 NANOPОWDERS
TiO2 based powders containing B2O3 and Nb2O5 were obtained through an aqueous sol-gel method. The as prepared gels were step wisely heated in the temperature range 200°C - 500°C and subsequently characterized by XRD, IR and UV-Vis analysis. The TiO2 (anatase) is the single crystalline phase which has been detected up to 500°C. Photocatalytic tests showed that the investigated samples possess photocatalytic activity toward Malachite green organic dye and TiO2/Nb2O5 exhibited higher photocatalytic activity than TiO2/B2O3 sample. The compositions exhibited good antimicrobial activity against E. coli NBIMCC K12 407 and Bacillus subtilis NBIMCC 3562.
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Journal of Chemical Technology and Metallurgy
Journal of Chemical Technology and Metallurgy Engineering-Industrial and Manufacturing Engineering
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