在连续流中对 N-Boc 保护胺进行选择性热解保护

IF 3.1 3区 化学 Q2 CHEMISTRY, APPLIED Organic Process Research & Development Pub Date : 2024-04-25 DOI:10.1021/acs.oprd.3c00498
Michelle-Rose Ryan, Denis Lynch, Stuart G. Collins* and Anita R. Maguire*, 
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引用次数: 0

摘要

在没有酸催化剂的情况下,一系列胺的 N-Boc 热脱保护反应可在连续流中轻松实现。虽然在甲醇或三氟乙醇中可以获得最佳效果,但在一系列不同极性的溶剂中也可以进行脱保护。通过温度控制,N-叔丁氧羰基的顺序选择性脱保护已得到证实,例如,在存在烷基 N-叔丁氧羰基的情况下,可有效去除芳基 N-叔丁氧羰基。作为一个原理证明,一个伸缩序列证明是成功的,该序列包括选择性地脱除 9h 中的一个芳基 N-Boc,然后进行苯甲酰化和脱除剩余的烷基 N-Boc,形成酰胺 13。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Selective Thermal Deprotection of N-Boc Protected Amines in Continuous Flow

Thermal N-Boc deprotection of a range of amines is readily effected in continuous flow, in the absence of an acid catalyst. While the optimum results were obtained in methanol or trifluoroethanol, deprotection can be effected in a range of solvents of different polarities. Sequential selective deprotection of N-Boc groups has been demonstrated through temperature control, as exemplified by effective removal of an aryl N-Boc group in the presence of an alkyl N-Boc group. As a proof of principle, a telescoped sequence involving selective deprotection of an aryl N-Boc group from 9h followed by benzoylation and deprotection of the remaining alkyl N-Boc group to form amide 13 proved successful.

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来源期刊
CiteScore
6.90
自引率
14.70%
发文量
251
审稿时长
2 months
期刊介绍: The journal Organic Process Research & Development serves as a communication tool between industrial chemists and chemists working in universities and research institutes. As such, it reports original work from the broad field of industrial process chemistry but also presents academic results that are relevant, or potentially relevant, to industrial applications. Process chemistry is the science that enables the safe, environmentally benign and ultimately economical manufacturing of organic compounds that are required in larger amounts to help address the needs of society. Consequently, the Journal encompasses every aspect of organic chemistry, including all aspects of catalysis, synthetic methodology development and synthetic strategy exploration, but also includes aspects from analytical and solid-state chemistry and chemical engineering, such as work-up tools,process safety, or flow-chemistry. The goal of development and optimization of chemical reactions and processes is their transfer to a larger scale; original work describing such studies and the actual implementation on scale is highly relevant to the journal. However, studies on new developments from either industry, research institutes or academia that have not yet been demonstrated on scale, but where an industrial utility can be expected and where the study has addressed important prerequisites for a scale-up and has given confidence into the reliability and practicality of the chemistry, also serve the mission of OPR&D as a communication tool between the different contributors to the field.
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