用扫描电子显微镜分析提取颗粒的尘埃粒度和粒度分布,并与光散射技术进行比较

IF 4.7 Q2 MATERIALS SCIENCE, BIOMATERIALS ACS Applied Bio Materials Pub Date : 2024-04-23 DOI:10.1002/ppap.202400032
A. Petersen, Jakob Wötzel, Christiane Zamponi, J. Kobus, Sebastian Wolf, F. Greiner
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引用次数: 0

摘要

本研究通过比较原位扫描电子显微镜(SEM)和基于米氏理论并利用神经网络进行评估的原位光散射法,对等离子体生长的纳米粒子的测量进行了研究。研究发现,粒度分布 (PSD) 正常且非常窄,支持单分散颗粒云的常见假设。重要的是,研究发现 PSD 的扩散范围与平均粒度成正比增加,这表明根据球形尘粒的半径不同,其生长率也不同。两种方法得出的结果一致,这鼓励在类似研究中使用无干扰、实时、基于光的米氏方法。
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Analyzing dust particle size and size distribution on extracted particles by SEM and comparing with light scattering techniques
This study investigates the measurement of plasma‐grown nanoparticles, comparing ex situ scanning electron microscopy (SEM) and an in situ light scattering method which is based on Mie theory and utilizes a neural network for evaluation. The research reveals that the particle size distribution (PSD) is normal and very narrow, supporting the common assumption of monodisperse particle clouds. Importantly, the study finds that the spread of the PSD increases proportionally with the mean size, suggesting varied growth rates based on the radius of the spherical dust grains. Both methods produce consistent results, which encourages the use of the interference‐free, real‐time, light‐based Mie method in similar studies.
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来源期刊
ACS Applied Bio Materials
ACS Applied Bio Materials Chemistry-Chemistry (all)
CiteScore
9.40
自引率
2.10%
发文量
464
期刊介绍: ACS Applied Bio Materials is an interdisciplinary journal publishing original research covering all aspects of biomaterials and biointerfaces including and beyond the traditional biosensing, biomedical and therapeutic applications. The journal is devoted to reports of new and original experimental and theoretical research of an applied nature that integrates knowledge in the areas of materials, engineering, physics, bioscience, and chemistry into important bio applications. The journal is specifically interested in work that addresses the relationship between structure and function and assesses the stability and degradation of materials under relevant environmental and biological conditions.
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