A. S. Konstantinov, A. P. Chizhikov, M. S. Antipov, P. M. Bazhin, N. Yu. Khomenko
{"title":"高温退火对基于 TiC/TiB2/Ti3SiC2 的复合材料结构和性能的影响","authors":"A. S. Konstantinov, A. P. Chizhikov, M. S. Antipov, P. M. Bazhin, N. Yu. Khomenko","doi":"10.1007/s11148-024-00867-9","DOIUrl":null,"url":null,"abstract":"<p>High-temperature annealing of a composite material based on the Ti<sub>3</sub>SiC<sub>2</sub> MAX-phase dispersion-strengthened with TiC and TiB<sub>2</sub> particles obtained by free SHS compression was carried out. The annealing was carried out in an oxidizing atmosphere at 900, 1100, and 1300°C for 10 h and at 1400°C for 4 h. Experimental dependences of the specific weight gain of the oxidized samples and the oxidation rate on the temperature and annealing time were plotted. The effect of annealing temperature on the phase composition, structure, and mechanical properties of the materials was established based on x-ray phase analysis, scanning electron microscope images, and energy-dispersive analysis. The proportion of the MAX-phase increased from 26 to 63 wt.% as the annealing temperature of the material increased.</p>","PeriodicalId":751,"journal":{"name":"Refractories and Industrial Ceramics","volume":null,"pages":null},"PeriodicalIF":0.4000,"publicationDate":"2024-05-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of High-Temperature Annealing on the Structure and Properties of a Composite Material Based on TiC/TiB2/Ti3SiC2\",\"authors\":\"A. S. Konstantinov, A. P. Chizhikov, M. S. Antipov, P. M. Bazhin, N. Yu. Khomenko\",\"doi\":\"10.1007/s11148-024-00867-9\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>High-temperature annealing of a composite material based on the Ti<sub>3</sub>SiC<sub>2</sub> MAX-phase dispersion-strengthened with TiC and TiB<sub>2</sub> particles obtained by free SHS compression was carried out. The annealing was carried out in an oxidizing atmosphere at 900, 1100, and 1300°C for 10 h and at 1400°C for 4 h. Experimental dependences of the specific weight gain of the oxidized samples and the oxidation rate on the temperature and annealing time were plotted. The effect of annealing temperature on the phase composition, structure, and mechanical properties of the materials was established based on x-ray phase analysis, scanning electron microscope images, and energy-dispersive analysis. The proportion of the MAX-phase increased from 26 to 63 wt.% as the annealing temperature of the material increased.</p>\",\"PeriodicalId\":751,\"journal\":{\"name\":\"Refractories and Industrial Ceramics\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.4000,\"publicationDate\":\"2024-05-13\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Refractories and Industrial Ceramics\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1007/s11148-024-00867-9\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Refractories and Industrial Ceramics","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1007/s11148-024-00867-9","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Effect of High-Temperature Annealing on the Structure and Properties of a Composite Material Based on TiC/TiB2/Ti3SiC2
High-temperature annealing of a composite material based on the Ti3SiC2 MAX-phase dispersion-strengthened with TiC and TiB2 particles obtained by free SHS compression was carried out. The annealing was carried out in an oxidizing atmosphere at 900, 1100, and 1300°C for 10 h and at 1400°C for 4 h. Experimental dependences of the specific weight gain of the oxidized samples and the oxidation rate on the temperature and annealing time were plotted. The effect of annealing temperature on the phase composition, structure, and mechanical properties of the materials was established based on x-ray phase analysis, scanning electron microscope images, and energy-dispersive analysis. The proportion of the MAX-phase increased from 26 to 63 wt.% as the annealing temperature of the material increased.
期刊介绍：
Refractories and Industrial Ceramics publishes peer-reviewed articles on the latest developments and discoveries in the field of refractory materials and ceramics, focusing on the practical aspects of their production and use.
Topics covered include:
Scientific Research;
Raw Materials;
Production;
Equipment;
Heat Engineering;
Applications.
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